GCMS quantitation results for sample AE10241, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020509\10241.D Vial: 19 Acq On : 10 May 2002 4:25 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Ethyl 2,3-dimethyl-l ,3-oxaz... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 33.84 0.67 ug/1 83417 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl 2,3-dimethyl-l,3-oxazolidi... 187 C9H17NO3 1000139-26-8 56 2 Butanamide, 2 - (dimethylamino)-N-.. . 556 C33H40N4O4 055517-68-5 50 3 Morpholine, 4-[3-(4-butoxyphenox... 293 C17H27NO3 000140-65-8 40 4 tanamide, 2-(dimethylamino)-N-... 593 C35H39N5O4 018397-13-2 39 Abundance Scan 5235 (33.838 min): 10241 ,D (-5221) (-) m/z 100.10 100.00% 100

5000 -—

55 33.60 33.80 34.00 34.20 126 170 212 255 ‘-‘T11 r... I_ 1 T 1 m/z 101.10 7.02% m/z—> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #43672: Ethyl 2,3-dimethyl-1,3-oxazolidine-2-acetate 100

5000 1 1 i ■ ■ 33.60 33.80 34.00 34.20 58 m/ z 55.00 6.48%

/z—> +24 0 50 144172 - 100 1K) 200 250 300 350 400 450 500 550 Abundance #43784: Butanamide, 2-(dimethylamino)-N-[5,8-dioxo-3-pheny... 100 LAAAAdLAd 33.60 33.80 34.00 34.20 5000 m/z 41.10 6.34%

n/z-> Abundance 42 70 , T"r **44 —4 150 0 50 100 100 131 175201226 263 293 200 ' 250 300 338 373 414440 350 400 450 #118666: Morpholine, 4-[3-(4-butoxyphenoxy)propyl]- 513 500 556 550 1nallale"nMAMA m/z 43.10 1 33.60 33.80 34.00 34.20 5.57% 128 5000

41 70

m/z—> 0 151111, 50 4 100 । 166.. 236 .293........ 150 200 250 300 350 400 450 500 550 33.60 33.80 34.00 34.20

10241.D SCAN020507.M Tue May 14 14:25:38 2002 Page 6

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