GCMS analysis results, sample AE11157, May 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020515\11157.D Vial: 9 Acq On : 15 May 2002 7:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 5 R.T.« EstConc Area Relative to. ISTD R.T. 31.95 0.29 ug/1 31767 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 74 2 Phenanthrene-d10 188 C14D10 001517-22-2 59 3 Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N20 035496-19-6 43 4 3-^mino-4-methyl-6-methoxyquinoline 188 C11H12N20 1000213-71-3 42 Abundan Scan 4914 (31.952 min): 11157.D (-4908) (-) m/z 188.15 100.00% 188

5000 94 - 132 160 mfe-> 42 78 ’ ’13 otelapandjaBhapana 12,1 ■ ■ । ■ ■ ■ ■ । 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ■ i ■ ■ ■ ■ i ■ " > । । ‘ । 315 । ' 31.60 31.80 32.00 32.20 m/z 94.10 28.48% Abundance #79826: Anthracene-d1 0- 188

5000 31.60 31.80 32.00 32.20 m/z 184.05 12.25% 8094 160

iz-> 20 30 ■ ‘11' '' ■ i'1 40 52,664 X+11813214644— 1 r 1'11111 ■ P " 1111111 " *111 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79827: Phenanthrene-d10 188 + 31.60 31.80 32.00 32.20 5000 m/z 160.30 11.76%

80 94 160 30 TTT—IIT 52,66. +.1108,1321464 nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #79716: -(4-Tolyl)-3-methyl-pyrazol-5-one 188 31.60 31.80 32.00 32.20 91 m/z 187.20 11.76% 105 5000 119 65 41 _L 146 ■ i " ' ■ i "* । i । i ' ' ' । ' 1111211151111100’1001——’ m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.60 31.80 32.00 32.20

11157.D SCAN020507.M Thu May 16 09:39:02 2002 Page 8

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