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GCMS analysis results for sample AE08253, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08253 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047830–000047850

Folder label: “GCMS X 4/8/02 A 4/17/02

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Scanned page image, NYC-WTC_000047842
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08253.D Vial: 11 Acq On : 17 Apr 2002 5:42 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 4 Morpholine, 4-methyl- Concentration Rank 9

R. T. EstConc Area Relative to ISTD R.T. 6.04 0.26 ug/L 280132 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 2 Oxirane, [(1-methylethoxy)methyl ]- 116 C6H1202 004016-14-2 9 3 2-Pentanone, 4-hydroxy-4-methyl - 116 C6H12O2 000123-42-2 9 4 Ethanol, 1-methoxy-, acetate 118 C5H10O3 004382-77-8 9

X_ Abundance Scan 504 (6.040 min): 08253. D (-499) (-) m/ z 43.00 100.00% 4

59 5000 WAA/WN A W—N—A , 101 I 1 ' 1 ' 1 1 1 1 ' I 1 ' 1 ' I ' 1 1 "I 1...... 49 5.60 5.80 6.00 6.20 6.40

m/z-> 0 36.—l 1,0 , Il |I, , 1 ' i 1 1 1 ' i ' ' 1 1 1 1 1 - i ■ ■ ■ ■ i ■ ■ - ■ । i + m/z 59.10 50.90% 10 20 30 40 50 60 70 80 90 100 110 Abundance #4714: Morpholine, 4-methyl- 43

5000 ..... ... ......... 5.60 5.80 6.00 6.20 6.40 101 m/z 58.10 22.48% 15 71 27

m/z-> 01 ......... 10 20 1111/3032, 38,140 | 49 56 62 l i I |

50 i I* I I |

60 i r i I | 77 |

70 I' I" I i |

80 i I 86 I I |—f— I

90 I I

100 , | I i I I

110 | I

Abundance #109751: Oxirane, [(l-methylethoxy)methyl]- 43 59 29 5.60 5.80 6.00 6.20 6.40 5000 m/z 101.00 19.40% 101 73

m/z-> 01 ... 10 r..... 20 । — 30 40 34 50 60 P4 | 70 80 | 86 ■ i ■ I ■ ' i ' < J 1 l-i ■ ■ ■ i • . . . । , 90 100 110 Abundance #109755: 2-Pentanone, 4-hydroxy-4-methyl- 1 I ' 1 43 5.60 5.80 6.00 6.20 6.40 m/Z 39.10 12.47%

5000 59

15 101 0 2931 ,38,, 1+ I 1 1 ■ ■ i ' ■ 1 ■ i 831'' 1 ' i 1 ■ ■ 1, i 1 1 1 1 1 1 1 53 , 5.60 5 80 6.00 6.20 6407 m/z-> 10 20 30 40 50 60 70 80 90 100 110

08253.D 041702SCAN.M Fri Apr 19 08:38:00 2002 Page 9

NYC-WTC_000047842

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