GCMS analysis results sample AE08486, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\02 0419\0 84 83.D Vial: 20 Acq On : 20 Apr 2002 2:50 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.16 12.00 ug/1 16220900 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentahone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 53 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 38 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 4 Propanoic acid, 2-nitro-, methyl... 133 C4H7NO4 006118-50-9 9 Abundance Scan 524 (6.158 min): 08483.D (-520) (-) m/ z 43.10 100.00% 43 59 5000 101 • ■ । ■ i • 1 1 * । * 1 1; ।1 1 1 11 1 5.80 6.00 6.20 6.40 6.60 -374 +53 .67 77 83 I* ‘**Is*‘‘I*‘‘II ,112 m/z 59.10 52.48% mfz~> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #109755:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 ■ ■ i ■ ■ ■ > i ■ 1 ■ ■ i ■ ■ • • i 1 1 1 1 i 1 59 5.80 6.00 6.20 6.40 6.60 m/z 101.10 20.74% 15 101

niz->______ 10 LX 20 253] ,37,1 +53 I • ■ ■ ■ i '1111 831,111 11 111. 1I 1 1 1 1 I 1 ‘ 11111111 ( 30 40 50 60 70 80 90 100 110 120 130 Abundance #109756:2-Pentanone, 4-hydroxy-4-methyl- 43 111’1414*1 Itrm । 5.80 6.00 6.20 6.40 6.60 5000 59 m/z 58.10 19.65%

. ........ . 37,1 I ________ 8 93 93 M 101 I_______________ -4’414 1 * * 111 ■ • • ■ । 1 1117 I '' ' ■ i • ■ ■ ■ i ■ ■ ■ ‘ i ■ ■ ■11 ■ ■ ■ ■ i 1 11 1 r11 11111 iz—>______ 10 20 30 40 50 60 70 80 90 100 110 120 130 _______________________ Abundance #4714: Morpholine, 4-methyl- 43 5.80 6.00 6.20 6.40 6.60 m/z 41.15 7.29% 50001

15 101 71

n/z—> +3, 10 | 49 56 62 77 86 —11100 ■ ■ ■ 11 ■ ■ ■ ।111 ■ ।'11111' 2030405060708090 100 110 120 130 5.806.001 6.20 6.406.60

08483.D SCAN020418.M Thu May 02 11:44:56 2002 Page 4

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