GCMS analysis results for sample AE06335, April 2002

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Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020408\6335.D Vial: 19 Acq On 9 Apr 2002 3:37 am Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C: \MSDCHEM\1. . . \SCANAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Morpholine Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 3.51 0.12 ug/1 149521 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Morpholine 87 C4H9NO 000110-91-8 4 2 Morpholine 87 C4H9NO 000110-91-8 4 3 cis-l-Nitro-l-propene 87 C3H5NO2 027675-36-1 4 4 Propane, 1,1-dimethoxy-2-methyl- 118 C6H14O2 041632-89-7 4 Abundance ’ Scan 74 (3.514 min): 6335.D (-65) (-) m/z 75.10 100.00% 75

5000 87

47 3.20 3.40 3.60 3.80 ' 4° 0 TIUTIUm mmmp " 11 ”' I " i " '1111' m/z 87.10 45.21% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #473: Morpholine 29 517

5000 87 1 I ■ ' ■ ' I • > 1 1 i 1 1 1 ' i 3 20 3.40 3.60 3.80 42 m/z 86.00 18.41%

m/z—> Abundance O+ ‘TI‘T‘‘‘EEIIIIEEI‘ITITT 133,.39445..5154 6063 68 73 7780 84 , Tuugug 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 w/wowo. #108086: Morpholine 29 57 87 1 '"I ' 1 1 1 1 320 3.40 3.60 3.80 5000 m/ z 47.05 14.84%

m/z-> 01 ....... ................ 3235,394345485154 ,606366 7073 7780 84 +....... TT I I| I I I I] I ■ I > I I II I | 1 I1 I | ! II I J y pN 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1244: cis-1-Nitro-1-propene ' ' I ’ ITII 39 320 3.40 3.60 3.80 m/ Z 40.10 Ww—WRAP 4.07% 5000 42

30 70 87 15 19 26 1 I 146 525558 73 I —HHH 5 mPH 0 rd | I I I t | I T TITHT .................. ... 1 • ’ ■ l • ■ < ■ I > ■ ■ ■ l m/z—> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 30 95 3.20 3.40 3.60 3.80

6335.D SCANAPR0902.M Tue Apr 09 15:21:19 2002 Page 5

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