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GCMS analysis results for sample AE06335, April 2002

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Laboratory report documenting GCMS analysis of sample AE06335 conducted on April 18, 2002.

NYC-WTC_000039405–000039416

Folder label: “GCMS X 3/18/02 A 4/8/02

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Scanned page image, NYC-WTC_000039415
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C : \MSDCHEM\1\DATA\020408\6335.D Vial: 19 Acq On 9 Apr 2002 3:37 am Operator: McLean Sample 3/18 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l..-\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

31.14 0.11 ug/1 227158 Phenanthrene-dl0 30.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 83 2 Phenanthrene-diO 188 C14D10 001517-22-2 9 3 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 9 4 Pentacyclo[7.3,1.1. (4,12) .0 (2,7) ... 188 C14H20 1000215-61-8 9 Abundance Scan 4775 (31.135 min): 6335.D (-4763) (-) m/z 188.10 100.00% US

5000 —.........., 80 94 30.80 31.00 31.20 31.40 O-TTTPPTTTTTTTT I"'‘I 11—1111—0011—1—TTUIEII‘tET11111117111I"I1" m/z 184.10 18.22% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- its

5000 +..... 30.80 31.00 31.20 31,40 m/z .94.10 17.49% 80 94 160 . . 17 30 42 52 66 108 118 132 146 || 170179 0 TDTImpog’uuurthr 'I"1'!"11 T I ] t t 1 I | l t I ! [ l t "I....... m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 US TIp—m—n—nBom I , T r-r-j , , , . । f 30.80 31.00 31.20 31.40 5000 m/z 189.10 16.09%

80 94 160 30 42 52 66 +108118.132,146170179—. 0 111'' I'1111 " '1 1111' 111 " I'11'!'' N ।'' miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79714: Pentacyclo[8.4.0.0(3,7).0(4,14).0(6,11)]tetradecane its 30.80 31.00 31.20 31.40 m/z .80.10 13.56%

5000 79 91

m/z-> 27 55 67 i| — ,l l „l 41 0 —7....... ----- 106 i I1! . 117 131 145

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 159 +173

30.80 31.00 31.20 31.40

6335.D SCANAPR0902 .M Tue Apr 09 15:21:19 2002 Page 6

NYC-WTC_000039415

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NYC-WTC_000039415Source: NYC Law Department, mirrored locally

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