GCMS analysis results for sample AE06336, April 2002

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Laboratory report documenting GCMS analysis of sample AE06336 conducted on April 18, 2002.

NYC-WTC_000039426–000039436

Folder label: “GCMS X 3/18/02 A 4/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020408\6336.D Vial: 20 Acq On 9 Apr 2002 4:33 am Operator: McLean Sample 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.14 0.11 ug/1 263209 Phenanthrene-dl0 3 0.92 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 90 2 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 78 3 Phenanthrene-diO 188 C14D10 001517-22-2 78 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N20 1000213-71-3 9 Abundance Scan 4776 (31.141 min): 6336.D (-4765) (-) m/z 188.10 100.00% 188

5000

40 80 94 30.80 31.00 31.20 31.40 O-P I ‘“ I " " 11 " " i' " r ■ " i" " i m/z 40.00 22.23% miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d1 0- 188

5000 30.80 31.00 31.20 31.40 m/z 94.10 17.98% „ 80 94 160 । 17 30 42 52 ° p J 108118 132 146 ,1 170179 0-' 1111 ■ 11 >1 ■ 1111111111111111 ii 1111111 [ 1111 [ 111111111111111 > 1111 i-i 11111 r> 111TTT 111111111TT1T11! m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance' #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )tetradeca... 188

30'30 31.00 31.20 31.40 5000 79 91 m/z 189.10 14.28% 55 67 105 117 131

Tl/Z-> —............. .. 0- 'I|•l>I'T|.. > > I >. >. I i l l. [. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 H 15,1173. Abundance #79827: Phenanthrene-d10 • ■ I ■ > ■ i l ■ • r. । ' 1 । । । 1 ' ' । j > 188 30.80 31.00 31.20 31.40 m/z 80.00 13.41% 5000

160 80 94 30 42 52 66 108 118 132 146 ,|| 170179,1,1 | m/z-> 0 I I I I I I I I I I I I I TT I I I I I I I I I I I I I I I I I t I I I TIr 11TTHTTTTTTTTTT 10 20 30 40 50 60 70 SO 90 100 110 120 130 140 150 160 170 180 190 4 30.80 31.00 31.20 31.40

6336.D SCANAPR0902.M Tue Apr 09 15:22:15 2002 Page 5

NYC-WTC_000039435

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NYC-WTC_000039435Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE06335, April 2002 · Box DEP Box 23

NYC-WTC_000039405

Laboratory report documenting GCMS analysis of sample AE06335 conducted on April 18, 2002.

1 shared topics · Same agency, volume and box · similarity 0.998