GCMS analysis results for sample AE06336, April 2002

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Laboratory report documenting GCMS analysis of sample AE06336 conducted on April 18, 2002.

NYC-WTC_000039426–000039436

Folder label: “GCMS X 3/18/02 A 4/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020408\6336.D Vial: 20 Acq On 9 Apr 2002 4:33 am Operator: McLean Sample 3/18 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 2 Acetonitrile, dichloro Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 3.31 0.13 ug/1 200867 1,4-Dichlorobenzene-d4 10.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 9 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 4 3 1H-Imidazole, 1-methyl- 82 C4H6N2 000616-47-7 3 4 Furan, 3-methyl- 82 C5H60 000930-27-8 2 Abundance Scan 39 (3.308 min): 6336.- (-37) (-) m/z 74 .00 100.00% 74 82

35 5000 49 '1 r ' " । " " ................. .. t-t| 1111111111 3.20 3.30 3.40 3.50 3.60 3.70 01 ■ 1 । 1 ■ ’ 1 । ' ■ ■ ■ । 1 1 1 1 i 1 1 1 ' r1 ' 1111 । । -i । । ■ ■ i 1 T-r-r-r-r-r-j-T-r-rr-p 1BTT m/ z 82.00 76.49% n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 T-rp-r TIT 1’11 1T ‘I0———11—11T 3.20 3.30 3.40 3.50 3.60 3.70 47 m/z 84.00 51.68% Ot 1 1 i 1 i 1 1 1 1 i 1 11 — r-j-r ‘Il 1 • l ■ ■ 1 ■ I 1 1 1 1 l > > ■ I I m/z— > 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74 III r-. . | I I I I | ri I I T’T I I | I I I I | I I i i । 3.20 3 30 3.40 3.50 3.60 3.70 5000 82 m/ z 35.10 51.21% 47 35 12 01 1 1 I 11 1 ' I 1 -26, ill , .. . —2—1 118 ।I ' l ■ ■ 1 1 I 1 i 108 * >■I ' 1 1 1 1 miz-> 10 20। 30 40 50 60 70 80 90 100 110 Abundance #116273:1 H-Imidazole, 1-methyl- ■rpn 1‘0‘T11.——11—TTIT 82 3.20 3.30 3.40 3.50 3.60 3.70 m/ z 49.10 30.04% 5000

42 54 .36., I _ L 67............ | 0 T-r-j-T-T-T-T-pi-T-r-T-y-r i i 11 ‘i‘i i i [111 1r -r-r-p-T-r-r i < , i , । n-rry , q-n-rr-j r, v. I , , "II" 1111’ " 1 1 ' 1 " I m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.30 3.40 3.50 3.60 3.70

6336.D SCANAPR0902.M Tue.Apr 09 15:22:13 2002 Page 4

NYC-WTC_000039434

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GCMS analysis results for sample AE06335, April 2002 · Box DEP Box 23

NYC-WTC_000039405

Laboratory report documenting GCMS analysis of sample AE06335 conducted on April 18, 2002.

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