GCMS analysis results, sample AE09155, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\050902\9155.D Vial: 20 Acq On : 10 May 2002 7:36 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 1 Acetonitrile, dichloro- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 3.59 0.25 ug/L 207235 1,4-Dichlorobenzene-d4 9.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-086 2 Acetonitrile, dichloro­ 109 C2HC12N 003018-12-0 9 3 Ethyl ether 74 C4H10O 000060-29-7 4 4 Acetic acid, dichloro-, ethyl ester 156 C4H6C12O2 000535-15-9 4 Abundance Scan 87 (3.590 min): 9155.D (-82) (-) m/z 74.00 100.00%| 74

5000 82

35 47 3.20 ... MS....... 3.40 3.60 3.80 4.00 0- ‘ ' I ' ' ' ' I ‘ ‘ ' I ' ‘ ' I ' ' I ' 1 ' 1155......... 1 ■ I111 ■ r ^ ’'' i1 88................. I ’ I ' । i ' I ' ' 1 ■ I ■ ' । ' I m/ z 82.00 48.60% n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 A 47 3.20 3.40 3.60 3.80 4.00 m/z 84.00 38.12% 35

n/z-> 0- 0 ' 1 1 1 10 12 20 26 30 L 11 -T-rI t‘l‘l i 1 ■ 1 1 i ■ 40 50 , 62....... 1 ■ i ■ ' ■ ■ i ■ 60 8070 ,i ■

90 i ■ ■ ■ 108l ■ ■ ■ i ■

100 110 ■ ■ 1 ■ ■ i M/Mmy Abundance #115342: Acetonitrile, dichloro- 74 35 3.20 3.40 3.60 3.80 4.00 5000 82 m/z 76.00 30.21% 47 - 0- t _____________ L 1 I ' ’ ' 1 I ' ‘it 1 ■ i ■ ■ ■ ■ i ■ ■1 ■ i ■ ■ ■' ।

m/z-> 0 10 20 30 40 5060 70 80 90 100 110 Abundance 31 #1050: Ethyl ether 3.20 ..... /'ll.......... 3.40 3.60 3.80 4.00 m/z 47.05 21.98%| 5000 59 45 15 74 MAMWMM

n/z-> 0 ..211 0 10 —2 TI 20 30 39, I, 40 50 'I 111 11 1 60 70 ■ ■ i

80 - ■ ■ ■

90 i ■ ■ ■ - i

100 ■ ■ ■ ■

110 i ■ ■ ■ ■ ।

320 3.40 3.60 3.80 4.00

9155.D 050102.M Mon May 13 11:41:46 2002 Page 4

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