GCMS analysis results for sample AE06306, April 2002

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Library Search Compound Report Data File C:\MSDCHEM\l\DATA\020408\6306.D Vial: 14 Acq On 8 Apr 2002 10:58 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

3.29 0.22 ug/1 164105 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 2 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 2 3 Chloromethyl ethanoate 108 C3H5C102 1000143-34-6 2 4 Ethanol, 2,2-dichloro- 114 C2H4C12O 000598-38-9 1 Abundance 1 Scan 36 (3.290 min): 6306.D (-23) (-) m/z 49.10 100.00% 43 49

74 84 ACMe 5000

3.20 3.30 3.40 3.50 3.60 3.70 o! TETT11ETr1111111/1/171 T ' I ' • ' ' | r i i 1 | । ■ 1 i ■ 1 i ' 1 ' 1 [d 1T } ' 1 ’ i m/z43.10 90.96% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 ■ ■ i ■' I11 " I ■" 11111111111111 3.20 3.30 3.40 3.50 3.60 3.70 47 m/ z 74.10 60.97% 01 ■ ■ i ■ 1 ' 1 1 1 1 1 1 1 1 1 1 — 1 ■ i ■ ■ ■ • i > > 1 > । ■ ■ > < । Till m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74 -n-p-r 1 rp-1-n p m-p-n-rp r 3.20 3.30 3.40 3.50 3.60 3.70 5000 82 m/z 34.00 55.68%

Of 35 .. 1012....20 26,301.40, L 50 47

, 62....... 1 . 108 A/"MMM T!I 1 1 1 1 ' 1 1 1 TT——TTTT m/z-> 60 80 70 90 100 110 Abundance #4957: Chloromethyl ethanoate 43 3.20 3.30 3.40 3.50 3.60 3.70 m/z 47.00 55.24% 5000 . MMvN N 49

0 - ‘II ■ ' i ’ 1 ' ' i ' 1 1 ■ i ' ■ ' ' i ■ ■ ' ■ i ■ ■ ' 1 i ■ ■ ■ 1 i 1 1 । 1 i T’T m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.30 3.40 3.50 3.60 3.70

6306.D SCANAPR0902.M Tue Apr 09 15:16:52 2002 Page 3

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