GCMS analysis results for sample AE06306, April 2002

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Laboratory report documenting GCMS analysis of sample AE06306 conducted on April 18, 2002.

NYC-WTC_000039363–000039372

Folder label: “GCMS X 3/18/02 A 4/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\DATA\020408\6306.D Vial: 14 Acq On 8 Apr 2002 10:58 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 2 HH-Dibenzo [b, E] [1,4] diazep. . . Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.69 0.15 ug/1 146723 Naphthalene-d8 15.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 HH-Dibenzo [b,E] [1,4] diazepin-ll. . . 267 C16H17N3O 013450-73-2 2 2 Ethyl 4-chloro-3-trifluoromethyl ... 267 C10H9C1F3NO2 018585-06-3 2 3 Benzoic acid, 2-[ (trimethylsilyl.. . 282 C13H2203Si2 003789-85-3 2 4 Stearic acid, 2-hydroxy-1-methyl... 356 C22H4403 014251-39-9 1 Abundance Scan 1976 (14.689 min): 6306.D (-1968) (-) m/ z 73.10 100.00% 73

5000 267 355 ■ 1 I ' 1 ■ ■ l ■ ■ T I 1 1 1 ' I ' ' 40 14.40 14.60 14.80 15.00 0- r 1111 r '11111'1 p " ■ r ' ■ ■ r ''' p " ' i r 111 r 11 r '" i ■' " i ■ ■ ■ ■ r ■ ■ ■ r " ■ i11 ‘ ‘ r m/z 267.00 37.17% m/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 y Abundance #955:11H-Dibenzo[b,E][1,4]diazepin-11-one, 5-(3-aminoprop... 30 1 8 57 77 181 267 223

5000 249 14.40 14.60 14.80 15.00 >7 154 m/ z 355.00 36.02% 0- i1'" ।1 | y 435, a । A , L 2 C — .'11................................. ' i11111" '1111111'1" I' ‘111' miz—> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #637: Ethyl 4-chloro-3-trifluoromethylcarbanilate 23

14.40 14.60 14.80 15.00 5000 195 m/z 40.10 11.80% 221 267 4 0- Th .450144 88.113 4447175. | 11TT THr Ti 248 ' i'1' ■ i " " i ■1' ‘ i " " i11 " i' m/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115268: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethyl... 73 14.40 14.60 14.80 15.00

5000 267

m/z-> 0 —2028.1 0 91,115 135152.175 193209.233250... "I ' rT P ' I I I ' 1 ' 'I ' ' 11 | ‘ I ‘ । । । । iryi i n | i 11 I I I I I' 11 I ri I |TTti 1’’’ ‘ i111' I ’1TTTTTT ' I' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360

6306.D SCANAPR0902.M Tue Apr 09 15:16:54 2002 Page 4

NYC-WTC_000039371

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Laboratory report documenting GCMS analysis of sample AE06336 conducted on April 18, 2002.

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