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← Document results/DEP Box 25/GCMS X 4/30/02 A 5/8/02
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GCMS analysis results for unknown compounds, sample AE10198, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10198 on May 10, 2002.

NYC-WTC_000044885–000044901

Folder label: “GCMS X 4/30/02 A 5/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050802\10198.D Vial: 16 Acq On 9 May 2002 3:38 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 1H-3-Benzazepine-2-carboxyl... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 36.91 0.28 ug/L 248375 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1H-3-Benzazepine-2-carboxylic ac... 221 C11H11NO4 017639-47-3 9 2 [2-(4-Dimethylaminocinnamoyl )-5-... 329 C18H18BF2NO2 1000223-62/3 9 3 3- 2,4-Dichloro-6-ethyl-5-pyrimi... 299 C14H19C12N3 1000212-53-2 9 4 N-[2-(2-Propenyloxy-)-3,5-dibrom... 514 C17H13Br3N2O2 1000223/53-6 9 Abundance Scan 5759 (36.917 min): 10198.D (-5744) (-) m/z 221.00 <100.00%

M 147 221 73 49 429 281 356 ............ /.................... 5000 191

... 36.60 36.80 37.00 37.20 0 1"1J "11 I"1111" 11"1' I" " i I " ‘' I " " I m/z 147.10 95.27%

_A m/z—> 20 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #87875: 1 H-3-Benzazepine-2-carboxylic acid, 2,3,4,5-tetrah... 221 121 148 5000 w,...J 36.60 36.80 37.00 37.20 91 176 m/z 221.90 89.86%

0 ........ ■r r1 u i" I ■ - ‘I 1′117’ 111101 । p> r ' । i । i rp, . "‘ATt’T’ IT. | T- ’ « | i i | i | i| i ... | m/z-> 20 40 60 80 100120140160180200220 240 260 280 300 320 340 360 380 400 420 Abundance 1 #3543: [2-(4-Dimethylaminocinnamoyl)-5-methylphenoxy]diflu... 42 77 - 11 7111 11*‘ I 36.60 36.80 37.00 37.20 5000 m/ z 73.05 72.97% 107 130 155174 328 NM 0 , . 14 r'" r "' r ‘" I" " i" " i 209 235 264 285 309 WAN NY "MMA/AMA m/z-> 20 40 60 80 100120140160180 200 220 240 260280 300 320 340 360 380 400 420 Abundance #2410: 3-[2,4-Dichloro-6-ethyl-5-pyrimidinyl]-3-azabicyclo... 41 67 36.60 36.80 37.00 37.20 218 m/z 49.20 64.19% .1 5000 i

I ll j 86 , 109

141 166 191 264 299 +ppevsltily4M4Ma 244 . 0 TT -----**#*** 1 * + 11 *+ 11, T . . i | I . । . | . . . । | . I i i । i i i i । । i . . । i i i . [ m/z-> 20 40 60 80 100120140160180200220240260280300320340360380400420 36.60 36.80 37.00 37.20

10198.D 050102.M Thu May 09 13:35:28 2002 Page 11

NYC-WTC_000044900

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

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Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

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