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GCMS sample analysis results, AE11800, June 3, 2002

Machine-extracted title · confidence 100%

Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.

NYC-WTC_000012823–000012851

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\11800.D Vial: 7 Acq On : 22 May 2002 6:43 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 17 1-Monolinoleoylglycerol tri... Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 36.45 0.39 ug/L 160501 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethy... 498 C27H54O4Si2 054284-45-64 2 5H-Isoindolo[1,2-b][3]benzazepin... 355 C20H21NO5 055228-79-0 3 3 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 2 4 2-(2,4,6-Trinitrophenyl)-3-oxobu... 341 C12H11N309 015010-19-2 2 Abundance Scan 5679 (36.447 min): 11800.D (-5672) (-) m/z 73.05 / 100.00%

M. 73

355 5000 147 209 295 429

49 36.20 36.40 36.60 36.80 0- 1na ----- m/z 354.90 58.19% miz-> 50 100 150 200450 250 300 350 400 Abundance #27370: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 TII ■ ‘ i ■ ■ • ■ i ■ • 36.20 36.40 36.60 36.80 | 34 103 m/z 83.90 . 51.77%! 281 0- — h 44 +12 i _ 1205327,355.325.429483 177, 1. 249„ miz-> Abundance 50 100 150 200 250 300 350 400 #103467:5H-Isoindolo[1,2-b][3]benzazepin-5-one, 7,8,13,13... 450 M W 355

36.20 36.40 36.60 36.80 5000 163 m/z 209.00 46.90%|

192 326 | 0- 1*,**1’ *IU’ I ’ ‘ ‘ ‘ l * • ’ • I ‘ ‘ i' 1 1 ■ i ■ ■ ■ 1 i ■ ' 1 ' i nz-> 50 100 150 200 250 300 350 400 450 Abundance #128844: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... T T 355 36.20 36.40 36.60 36.80 m/z 295.00 45.58%

5000 73

147 0 ■ 45 ■11 • ■ L...... 1193 -H 267 295 384 42 457 1 1 i • ■ M ' ‘ I ‘ ‘ niz-> 50 100 150 200 250 300 350 400 450 36.20 36.40 36.60 36.80

11800.D 052202.M Tue May 28 12:04:47 2002 Page 20

NYC-WTC_000012847

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NYC-WTC_000012847Source: NYC Law Department, mirrored locally

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