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GCMS sample analysis results, AE11800, June 3, 2002

Machine-extracted title · confidence 100%

Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.

NYC-WTC_000012823–000012851

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\11800.D Vial: 7 Acq On : 22 May 2002 6:43 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan "6 Library : C:\DATABASE\NIST98.L Peak Number 18 2-Amino-2-oxo-acetic acid, . Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 37.70 0.33 ug/L 137877 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Amino-2-oxo-acetic acid, N-[3,... 221 C12H15NO3 1000127-85-3 5 2 6-Ethyl-5-[1-piperidinyl] -2,4-py... 221 C11H19N5 1000212-52-9 5 3 9H-Purin-6-amine, N-methyl-9-(tr... 221 C9H15N5Si 032865-83-2 4 4 1,3-Benzodioxole, 5-[3-acetamino... 221 C12H15NO3 1000124-33-0 4 Abundance Scan 5893 (37.704 min): 11800.D (-5883) (-) m/z 221.00 100.00% 221

73 147 5000 282 355 40 I ' 1 1 ' i ' ' ' ' I ■ ■ i 1 ■ ■ ‘ i ' '

miz-> 0- 40 + • i ■ ■ “ i •' I “ ■ ■ i“■■i■'■ ■ i■ ■ ■ • i 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■i■ 4 * I *'' * I ‘ ‘'4 f ‘ ‘ ‘ *.’**414 *’*1’’’’I’**’13 37.40 37.60 37.80 38.00 m/z 147.00 66.07% Abundance #87891:2-Amino-2-oxo-acetic acid, N-[3,4-dimethylphenyl]-... 221

147 5000 120 11 37.40 37.60 37.80 38.00 m/z 73.00 60.21% 77 105

A 11 ** +r* 14 4.44 — 165 193 | 0- ■ ■ i■ ■ ■ ■ i ■ i■'' ■ r1 ■ “ ।■ ■ ■ ■ । ■ i • • ■'i‘1 ■' i " "i■ ■ ■ • i ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #87832:6-Ethyl-5-[1-piperidinyl]-2,4-pyrimidinediamine 221 43 164 37.40 37.60 37.80 38.00 5000 m/z 355.00 32.33% 137 68 84 192 0 — J +4.419 4. Al a, ah 4 17 . । miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #87924: 9H-Purin-6-amine, N-methyl-9-(trimethylsily!)- ■ ■ i 1 ■ ■ ■ i ■ FI * * * 1 I > । * I 221 37.40 37.60 37.80 38.00 m/z 282.10 30.55% 73 206 5000

45 165 I I । 99 123138 । 191 0 r. |l-i ndh : w P mpnt d mpidihhijhi thh ■ mst । n ipa■ ■ i ■ • (. .... t.... 1.. i “ “ i ■ “ ■ i" " i “ “ i “ • ‘i ■ ’tt m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 37.40 37.60 37.80 38.00

11800.D 052202.M Tue May 28 12:04:48 2002 Page 21

NYC-WTC_000012848

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NYC-WTC_000012848Source: NYC Law Department, mirrored locally

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