NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\052202\11800.D Vial: 7
Acq On : 22 May 2002 6:43 pm Operator: Mclean
Sample : 5/21 ad Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan "6
Library : C:\DATABASE\NIST98.L
Peak Number 18 2-Amino-2-oxo-acetic acid, . Concentration Rank 19
R.T. EstConc Area Relative to ISTD R.T.
37.70 0.33 ug/L 137877 Perylene-d12 34.66
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Amino-2-oxo-acetic acid, N-[3,... 221 C12H15NO3 1000127-85-3 5
2 6-Ethyl-5-[1-piperidinyl] -2,4-py... 221 C11H19N5 1000212-52-9 5
3 9H-Purin-6-amine, N-methyl-9-(tr... 221 C9H15N5Si 032865-83-2 4
4 1,3-Benzodioxole, 5-[3-acetamino... 221 C12H15NO3 1000124-33-0 4
Abundance Scan 5893 (37.704 min): 11800.D (-5883) (-) m/z 221.00 100.00%
221
73 147
5000
282 355
40 I ' 1 1 ' i ' ' ' ' I
■ ■ i 1 ■ ■ ‘ i ' '
miz->
0-
40
+ • i ■ ■ “ i •' I “ ■ ■ i“■■i■'■ ■ i■ ■ ■ • i
60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
■i■ 4 * I *'' * I ‘ ‘'4 f ‘ ‘ ‘ *.’**414 *’*1’’’’I’**’13
37.40 37.60 37.80 38.00
m/z 147.00 66.07%
Abundance #87891:2-Amino-2-oxo-acetic acid, N-[3,4-dimethylphenyl]-...
221
147
5000 120 11
37.40 37.60 37.80 38.00
m/z 73.00 60.21%
77 105
A
11 ** +r* 14 4.44 — 165 193 |
0- ■ ■ i■ ■ ■ ■ i ■ i■'' ■ r1 ■ “ ।■ ■ ■ ■ । ■ i • • ■'i‘1 ■' i " "i■ ■ ■ • i ■
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
Abundance #87832:6-Ethyl-5-[1-piperidinyl]-2,4-pyrimidinediamine
221
43
164 37.40 37.60 37.80 38.00
5000 m/z 355.00 32.33%
137
68 84
192
0 — J +4.419 4. Al a, ah 4 17 . ।
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
Abundance #87924: 9H-Purin-6-amine, N-methyl-9-(trimethylsily!)- ■ ■ i 1 ■ ■ ■ i ■ FI * * * 1 I > । * I
221 37.40 37.60 37.80 38.00
m/z 282.10 30.55%
73 206
5000
45 165
I I । 99 123138 । 191
0 r. |l-i ndh : w P mpnt d mpidihhijhi thh ■ mst । n ipa■ ■ i ■ •
(. .... t.... 1..
i “ “ i ■ “ ■ i" " i “ “ i “ • ‘i ■ ’tt
m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 37.40 37.60 37.80 38.00
11800.D 052202.M Tue May 28 12:04:48 2002 Page 21
NYC-WTC_000012848
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