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GCMS analysis results for sample AE12162, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE12162 conducted on June 5, 2002.

NYC-WTC_000013643–000013665

Folder label: “GCMS X 5/22/02 A 5/23/02

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Scanned page image, NYC-WTC_000013663
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NYC 9/11 Public Portal Document Library Search Compound Report

$ Data File : C:\MSDCHEM\1\DATA\052302\12162.D Vial: 15 Acq On : 23 May 2002 9:22 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 3-Isopropoxy-l, 1,1,5,5,5-he... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

35.37 0.29 ug/L 79799 Perylene-d12 34.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,5,5,5-hexamet... 354 C12H3404Si4 072182-11-7 9 2 Silanamine, N-[2,6-dimethyl-4-[(... 281 C14H27NOSi2 072088-09-6 5 3 2-Amino-2-oxo-acetic acid, N-[3,... 221 C12H15NO3 1000127-85-3 5 4 2,4-Diamino-N,N,5-trimethyl-6-qu... 281 C11H15N5O2S 1000227-25-1 5 Abundance Scan 5496 (35.371 min): 12162.D (-5484) (-) m/z 73.10 100.00% 73 221 281 5000 147 355 44 3500 35.20 35.40 35.60 35.80 ------- 0- ■ ■ i ■ ■ ■ ■ i ■ ■ ■ • i ■ • ■ ■ i • ■ " i ■ ■ " 11' • ■ i ■ m/z 221.00 65.70% mz-> 40 60 80 100 120 140 160 180 2(X) 220 240 260 280 300 320 340 Abundance #27710:3-lsopropoxy-1,1,1,5,5,5-hexamethyI-3-(trimethylsi... 73 281

43

w 5000 207 339 35.00 35.20 35.40 35.60 35.80 m/z 281.00 57.05%

mz-> 01 4 . t... .133 163 . I. 129/— 249265 1’7’11+1444’7 14/k ’ ’’1’’*/11***1’**1’’I’’* TTTTTMa 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 I Abundance #27716: Silanamine, N-[2,6-dimethyl-4-[(trimethylsilyl)oxy... 1 73 281 ‘ ‘ 1* ' ‘ ‘ 1 ‘1 7'I ■ iI ■ 266 35.00 35.20 35.40 35.60 35.80 5000 m/z 147.00 46.35% 45 251 179 97 120 147 236 ,

n/z-> | 0- ।‘ ’ 15 | ‘ ‘ I •' HL4 III 1 ......... I ’!*111117710/1111137111T7317 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #87891:2-Amino-2-oxo-acetic acid, N-[3,4-dimethyIphenyl]-... 221 35.00 35.20 35.40 35.60 35.'80 m/z 207.00 32,60% 147 5000 120

77 105 m/z-> 0 —40HH+ 165 193 a I*B44,****p’’ 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.00 35.20 35.40 35.60 35.'80

12162.D 052202.M Wed May 29 09:55:13 2002 Page 16

NYC-WTC_000013663

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NYC-WTC_000013663Source: NYC Law Department, mirrored locally

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