GCMS analysis results for sample AE12162, June 2002

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Laboratory report documenting GCMS analysis of sample AE12162 conducted on June 5, 2002.

NYC-WTC_000013643–000013665

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\12162.D Vial: 15 Acq On : 23 May 2002 9:22 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 .gamma.-Cyano-3-methyl-5,10... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

34.82 0.84 ug/L 231525 Perylene-dl2 34.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 .gamma.-Cyano-3-methyl-5,10-dihy... 208 C14H12N2 1000213-00-8 7 2 2-Propen-1-one, 1,3-diphenyl- 208 C15H120 000094-41-7 7 3 Bendazol 208 C14H12N2 000621-72-7 7 4 Dibenzo [by E]-1,4-diazabicyclo [2 ... . 208 C14H12N2 094509-68-9 7 Abundance Scan 5402 (34.819 min): 12162.D (-5401) (-) m/z 117.90 100.00% 1* 8 281

86 208 5000 44 262 132 34.40 34.60 34.80 35.00 35.20 0! ■ ■ i ‘ • 1’1—0’117 I ‘ ' 4 ‘ I l”r ‘ ’ 4 4 1 1 ‘ 4 4 ‘ I ‘ ’ 4 4 1 ‘ ' ' i ‘ • 1 i • ‘ 1 • ! f 4 ‘ ' i ‘ 4 m/z 280.90 93.79% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #84850: ,gamma.-Cyano-3-methyl-5,10-dihydrobenzo[fJindolizine 193267 li An 5000 A 1 4 4 7 34.40 34.60 34.80 35.00 35.20 1 ‘II

103 m/z 208.00 58.82% , 128 151164 180 01 ‘1‘* —mp I ‘ 4 4 I 4 4 4 4 1 4 4 4 4 1 niz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #126479:2-Propen-1-one, 1,3-dipheny- 207

77 34.40 34.60 34.80 35.00 35.20 5000 m/z 85.90 58.50% 131 105 51 179 64. 99.4 28 ...... . 0 -H ‘ ‘ I ‘ ' I ‘ ‘ ■ I ‘ ‘ ‘ I ‘ ' miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #84873: Bendazol .... J MAAA# AAA MAM I ‘ 4 • 4 I 2017 34.40 34.60 34.80 35.00 35.20 m/z 207.00 52.29% 5000

65 91 104 131 ++ 4.117/111— 51 7R

miz—> 0- I** 20 4..4. 152 167180193 i 40 60 80 100 120 140 160 180 200 220 240 260 280 ‘ ■ i'' ■ ■ i1 ■ ■ ■ i ■ ■ ■11'1 34.40 34.60 34.80 35.00 35.20

12162.D 052202.M Wed May 29 09:55:13 2002 Page 15

NYC-WTC_000013662

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NYC-WTC_000013662Source: NYC Law Department, mirrored locally

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