GCMS sample analysis results, AE11800, June 3, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.

NYC-WTC_000012823–000012851

Folder label: “GCMS X 5-21-02 A 5-22-02”

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NYC 9/11 Public Portal Document Library Search Compound Report • . Data File : C:\MSDCHEM\1\DATA\052202\11800.D Vial: 7 Acq On : 22 May 2002 6:43 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 1-[2-Pyridylethanone]-2-[N(... Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T. 34.85 0.39 ug/L 161672 Perylene-dl2 34.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-[2-Pyridylethanone] -2-[N(l),N(... 245 C13H19N5 1000212-28-7 9 2 Bendazol 208 C14H12N2 000621-72-7/7 3 2-Propen-1-one, 1,3-diphenyl-, (E)- 208 C15H12O 000614-47-1 7 4 .gamma.-Cyano-3-methyl-5,10-dihy... 208 C14H12N2 1000213-00-8 7 Abundance Scan 5407 (34.849 min): 11800.D (-5405) (-) m/z 207.00 /100.00%

5000 44 129 2017 281

„ssps/tanpaeaptMN 260 221 34.60 34.80 35.00 35.20 0! I m/z 129.40 89.74% ■ । • ■ ■ • । • ■ ■ ■ । ■ ■ ■ ■ । • ■ । ■ ■ ■ ■ । ■ i ■ ‘ ‘ i ■ ■ ■ i ■' ■11 ■ • ■ ■ i ■ ■ miz-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #59850:1 -[2-Pyridylethanone]-2-[N(1 ),N(3)-dimethylhexahyd... 42 132 245

5000 55 69 84 114

167 230 _R 34.60 34.80 35.00 35.20 m/z 281.00 87.18% 0 i■■■•i1 44a— 4 152 . 'I Prttrrt 188 202216 14* p , ,■! । 1 1" . [ -n-p-r-n-p-r mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #84873: Bendazol 207 T • ■ i ' ' ■ ' i ' ' ' ' i ' ■ 34.60 34.80 35.00 35.20 5000 m/z 208.00 67.69%

65 91 103 51 77 O' 4. — 116 131 152 167180 193 1 miz-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 #85108:2-Propen-1-one, 1,3-diphenyl-, (E)- ILnRWbpAo" 77 208 34.60 34.80 35.00 35.20 m/z 44.10 53.85% 103 131 5000 51 179 89 165

m/z-> 27 39 0 TTgTT 4—4 20 40 60 80 63 L 115 rrt-p-r 152 I I li 191 i 4 11 n । r I* > 0r 'i * 100 120 140 160 180 200 ■ ■ i 1 ■ 111 * ‘ 220 240 260 280 ■ i ■11 ■ i * • 34.60 34.80 35.00 35.20

11800.D 052202.M Tue May 28 12:04:43 2002 Page 16

NYC-WTC_000012843

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GCMS sample analysis results, AE11907, June 4, 2002 · Box DEP Box 15

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.

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