NYC-WTC_000023904
Laboratory report showing GC/MS analysis of sample AE10981 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 22 pages
GCMS analysis results, sample AE09155, May 2002
Machine-extracted title · confidence 100%GCMS analytical report for environmental sample AE09155 including surrogate compound data from May 15, 2002.
NYC-WTC_000022857–000022878Folder label: “GCMS X 5/8/02 A 5/10/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\050902\9155.D Vial: 20 Acq On : 10 May 2002 7:36 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L
Peak Number 8 1’H-Estra-1,3,5(10),9(11)-t... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.
33.11 0.37 ug/L 188683 Perylene-dl2 34.70
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l'H-Estra-1,3,5(10),9(11)-tetrae... 297 C19H23NO2 013871-40-4 10 2 14.alpha.-Hydroxy-3-methoxy-D-ho... 314 C20H26O3 1000215-85-9 9 3 D-Homoestra-1,3,5(10)-trien-17a-... 314 C20H26O3 010003-04-0/9 4 Bendazol 208 C14H12N2 000621-72 7 7 Abundance Scan 5111 (33.109 min): 9155.D (-5107) (-) m/z 283.10 10 . 00% 283 429 149 207 49 73 355 5000
■ ‘ I ' 1 ' ' I ' ' 1 1 ' ' ' I 32.80 33.00 33.20 33.40 O- TTTp-rTrp-rrrp-rTTp-rTTpT-rrp-^^ I' FTITr 1 “ 11 r ‘111"111"111 *"11'111111" i m/z 429.10 90.22%
A I'1 "I m/z-> 40 60 80 100120140160180200220240260280300 320340360380400420 Abundance #99175:1 ’H-Estra-1,3,5(10),9(11 )-tetraeno 1,10,9,11 -bcdjp... 297
5000 186 32.80 33.00 33.20 33.40 160 m/z 149.20 82.67%
niz-> 0" । ■ i" " i"1' i" " i ■ ■" i ‘1 A , 224
40 60 80 100120140160180200220240260280300320340360380400420 267 111111110/11111111110271111111111711
Abundance #99006:14.alpha.-Hydroxy-3-methoxy-D-homoestra-1 l3>5(10)-... 186 296
314 ' ■ i ■ ' ■ ■ i ■ ■ ■ ■ i ■ • ■ ■ i 32.80 33.00 33.20 33.40 161 5000 127 m/z 207.05 80.00%
225
mfc-> 0 ’1141444**4144 .4 4444+ 268 mHmmmmHHHHHH
40 60 80 100120140160180200220240260280300320340360380400420 Abundance #99007: D-Homoestra-1,3,5(10)-trien-17a-one, 14-hydroxy-3-... 186 2916 32.80 33.00 33.20 33.40 314 m/z 297.20 76.44% 160 5000 127 91 225
n/z-> 4+4 0 ■ i"' ■ i ■"' i ■ ■ i I > 268 dhalghadhabapalanyann i" " i‘" ■ i i" ’1 r " ■ i" ■1 r“' i 40 60 80 100120140160180200220240260280300320340360380400420 32.80 33.00 33.20 33.40
9155.D 050102.M Mon May 13 11:41:47 2002 Page 11
NYC-WTC_000022872
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NYC-WTC_000022872Source: NYC Law Department, mirrored locally
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