GCMS analysis results, sample AE09155, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\DATA\050902\9155.D Vial: 20 Acq On : 10 May 2002 7:36 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 9 Acridine, 9,10-dihydro-9,9,... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

33.13 1.30 ug/L 671033 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acridine, 9,10-dihydro-9,9,10-tr... 223 C16H17N 025308-77-4 9/ 2 4-Quinolinol,4-ethenyl-1-ethylde... 223 C14H25NO 038463-59-1 9 3 1,3-Dithiane, 2-(phenylmethylene) 208 C11H12S2 1000196-75-2 7 4 Pyrimidine, 2-chloro-4-(4-fluoro... 208 C10H6C1FN2 085979-59-5 5 Abundance Scan 5114 (33.127 min): 9155.D (-5112) (-) m/z 208.00 100.00% 208 74 357 147 295 5000 36 430

• * i • ’ ■ i ' 32.80 33.00 33.20 33.40 01 m/z 74.10 71.36% m/z-> 50 100 150 200 250 300 350 400 Abundance #85143: Acridine, 9 10-dihydro-9,9,10-trimethyl- 208

5000 ' ' I ' ' ' ' I ' ' i ■ 1 ■ ■ i ■ 1 ■ 1 i 32.80 33.00 33.20 33.40 m/z 357.10 65.68% 27 51 77 194 139 165 188 , 01 11 r -1*Am-rhungi ‘ i41 । 1 "m ■ । । । । i । । ■ । । 4 miz-> 50 100 150 200 250 300 350 400 Abundance #85065:4-Quinolinol,4-etheny!-1 -ethyldecahydro-2-methyl-(... 208 ■ ■ i ■ ■ ■ ■ i ■ 1 * i 1 * * * i 1 * 1 * i 32.80 33.00 33.20 33.40 180 5000 55 m/z 147.10 52.59%

1 79 110 152 0- 11 un.il luh a4 Ah, d 'I Ml—L41—1— 11’’ ' I ' 1 ' 1 1 1 ' 1 ' 1 1 n/z-> 50 100 150 200 250 300 350 400 Abundance #85014:1,3-Dithiane, 2-(phenylmethy!ene) A................ * * I 1 ‘ 1 ’ I 208 32.80 33.00 33.20 33.40 134 m/z 295.10 47.41% 5000

115,411161180 90 , 0 26 45 69 ,1 ■ ' i ' ■ 1 ' i n/z-> 50 100 150 200 250 300 350 400 32.80 33.00 33.20 33.40

9155.D 050102.M Mon May 13 11:41:47 2002 Page 12

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