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GCMS analysis results for sample AE00165, Feb 2002

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Laboratory report listing unknown compounds and surrogate recovery for sample AE00165 analyzed on February 13, 2002.

NYC-WTC_000050664–000050682

Folder label: “GCMS X 1/4/02 A 2/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB04\00165.D Vial: 4 ' Acq On : 4 Feb 2002 5:37 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCANS08.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Acridine-D9 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.31 ug/L 249990 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acridine-D9 188 C13D9N 000000-00-0 72 2 Acridine-D9 188 C13D9N 000000-00-0 72 3 7-methoxy-5-methylnaphthalen-2-ol 188 C12H1202 000000-00-0 59 4 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 50 Abundance Scan 1699 (22.771 min): 00165. D (-) m/z 188.15 100.00% 188

5000

94 42 54 64 80 2240 22.60 22.80 23.00 23.20 ol THm +++ .■I....,.............. I’’ m/z 94.10 17.81% 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 1118

5000 _ ------- 22.40 22.60 22.80 23.00 23.20 93 m/z 189.20 15.05% 66 80 I, 158

niz-> ol 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .... A..- Abundance #85255: Acridine-D9 188

2240 22.60 22.80 23.00 23.20 5000 m/z 80.10 8.93% 93 158 66 80 . ol ■ ■ । ■ ■ ■ ■ । ■ — ................ r/ll/n.,.....Ill... m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #98127:7-methoxy-5-methylnaphthalen-2-ol . ।।. ।.... ।,,,. 1. 158 22.40 22.60 22.80 23.00 23.20 m/z 184.10 6.90%

5000 145 115 127 159

n/z-> 51 63 ..... 1... 1.......... ... 94 01 ■ 1 | .... । . 1 | I | 1', i I | .... j .... | I I I I | I . TTPTTWTITTTTLTTTTTTTTTTTTTTTTTTTT 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 U ,m 22.40 22.60 22.80 23.00 23.20

)0165.D SCAN508.M Tue Feb 05 09:47:35 2002 Page 14

NYC-WTC_000050681

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NYC-WTC_000050681Source: NYC Law Department, mirrored locally

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