GCMS analysis results, sample AE03616, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03616.D Vial: 6 * Acq On : 8 Mar 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.40 ug/L 385839 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 94 2 6,8A-DIMETHYL-9-METHYLIDEN-2,5-M... 188 C14H20 058651-05-1 58 3 Acridine-D9 188 C13D9N 000000-00-0 56 4 Acridine-D9 188 C13D9N 000000-00-0 50 Abundance Scan 1718 (22.768 min): 03516. D (-) m/z 188.10 100.00% 188

5000

94 22.40 22.60 22.80 23.00 ‘ ‘ ‘ ' miz-> 42 52 0- TT — 66 807 40 50 60 70 80 90 1 132 146 158 ,10 120 130 140 150 160 170 180 190 l m/z 94.00 15.06% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 k 188

5000 ................... 22.40 22.60 22.80 23.00 ‘ 80 94 m/z 189.10 14.02% 0- TIM—puTtr 66 158 I I TTTTt 1 ■ l1'11111'1' I'1 “ I“ "11,11’l"111" '111 +44 1111 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #98522: 6,8A-DIMETHYL-9-METHYLIDEN-2,5-METHANO-1,2,3,3A,4,... “ 188 . । . . . . । , r. i t t । r । । । i i i । । 96 105 22.40 22.60 22.80 23.00 5000 119 131 145 m/z 184.05 9.42% 79 159 173 65 0- ....... T.. I... . TIWTIWTTWTTTTIT miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85255: Acridine-D9 118 22.40 22.60 22.80 23.00.. m/z 80.00 8.22% 5000

S3 66 158 132 11 | 0- TTTITT TI - ■ i ■ • 1 ■ i ■ ■ ■ 1 i '' ' 1 1 i 1 1 1 1 i 1 mfz~> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00

03516.D HP022102.M Fri Mar 15 10:09:36 2002 Page 14

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