Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
NYC-WTC_000037780–000037799Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03616.D Vial: 6 Acq On : 8 Mar 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 N-perdeuteriobenzylideneani... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 124190 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual l N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 6 2 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0/ 2 3 1-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54— 50 4 Pyrazine, tetraethyl- (CAS) $$ t... 192 C12H20N2 038325- +5-8 42 _______ Abundance Scan 1675 (22.283 min): 03516.D (-) m/z 192.00 100.00% 192
5000
96 146 t । ■ । । । । 1 । — P - 160 22.00 22.20 22.40 22.60 0 42 70 82 120 n—TTTHHp TIWTT , ml m/z 191.00 17.96% miz—> 20 30 40 50 60 70 80 90 Its 110 120 130 140 150 160 170 180 ISO 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192
5000 82 ........... 4 22.00 22.20 22.40 22.60 54 110 m/z 96.00 17.17%
m/z—> T 30 Ofmmm Tmm TT 1 94 MH mmp 160 TT — — 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 L Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 77 151 - 4,, 130 22.00 22.20 22.40 22.60 93 104 5000 m/z 146.10 15.23% 119
177 I m/z—> 2"3 40"50"8878 '90'100 778 ‘120' 738 748188 780770 180 738 200 Abundance #101918:1 -amino-2-methy!-4-isopropyl-thiotriazaphospholin... Tf 159 192 22.00 22.20 22.40 22.60 m/z 193.00 14.24% 5000
144 177 0 T mm mp -P mmmmmm । > — m m/z—> 20 30 40 50 60 70 80 80 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60
03516.D HP022102.M Fri Mar 15 10:09:36 2002 Page 13
NYC-WTC_000037796
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NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006105
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03246 conducted on March 15, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.998
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NYC-WTC_000037604
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
Filed in the same folder
NYC-WTC_000037605
Record of water sample extraction parameters including drip rates, volumes, and pH measurements from February to March 2002.
Filed in the same folder
NYC-WTC_000037611
Reference standard analysis data verifying instrument performance for detecting volatile organic compounds in water samples.
Filed in the same folder
NYC-WTC_000037616
Laboratory report showing GCMS blank analysis results for volatile organic compounds with detection limits below MDL.
Filed in the same folder
NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
Filed in the same folder