GCMS analysis results for sample AD31646, Jan 25 2002

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Laboratory report documenting GCMS analysis of sample AD31646 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050240–000050257

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31646.D Vial: 2 Acq On : 22 Jan 2002 1:02 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.29 ug/L 153226 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 93 2 Anthracene-dlO- 188 C14D10 001719-06-8 93 3 Acridine-D9 188 C13D9N 000000-00-0 64 4 Cycloheptanone, 4 -phenyl - 188 C13H160 067688-28-2 47 Abundance Scan 1699 (22.771 min): 31646.D (-) m/z 188.10 100.00% 128

5000 ........... ...

49 66 80 94 160 22.40 22.60 22.80 23.00 23.20 ■ ■ i ■ I-11' l" mmpI|’’ m/z 94.05 15.93% nz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

■ । ■ . . > | — T"| I > > 1 | 1 । I I | I 5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.00 12.81%

nz-> 66 ■ ■ i ■ • ■ • i • i • > i • -1 • i ■ ■ ‘ 1 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 > > 1 * • ■ i J > > > 11 • i»«1 * * * *! •' >»t1 *1 * I' •1 ’ l • > -H Abundance #84502: Anthracene-d10- 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 189.10 11.21%

niz-> ........... ir... 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 118 22.40 22.60 22.80 23.00 23.20 m/z 184.10 9.74% 5000

66 80 33 ' ■ i ■ “ ■ i • ■ ■ • i ■ ‘1' i11 •11 ■1 ■ • ।1 *1 ■ i ■ ■ ■ ■ i ■ ■ ■ • i ‘ i ■' ■ ■ i 158 i( “ I' ■ ''"I * * • ■ ।' • • ■ ।' r 1’ ’ /z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

31646.D SCAN508.M Thu Jan 24 13:55:35 2002 Page 12

NYC-WTC_000050255

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NYC-WTC_000050255Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AD31647, Jan 25 2002 · Box DEP Box 28

NYC-WTC_000050205

Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.

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