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GCMS analysis results for sample AE00307, Jan 2002

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Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051055–000051072

Folder label: “GCMS X 1/7/02 A 1/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN08\307.D Vial: 6 Acq On : 8 Jan 2002 9:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.30 ug/L 157875 Phenant hrene-dlO 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Phenanthrene-dlO 188 C14D10 001517-22-2 72 3 Acridine-D9 188 C13D9N 000000-00-0 64 4 Anthracene-dlO- 188 C14D10 001719-06-8 64 Abundance Scan 1699 (22.771 min): 307.D (-) m/z 188.10 100.00% 188 N

5000

66 80 94 158 — ... 4—........ 22.40 22.60 22.80 23.00 23.20 49 0 I' 1'1 11 — ■ ■ 11.... | H......................... . ■ । ■ r. - m/ z 94.10 19.78% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/ z 80.00 15.49% 66 I 158 II‘lI , , , , 0 ।111 (। ■'' । mfrptr PPr Fr | I I I I | I ! I I | I I I I | I I I I | I I I I | I I I l'| > Pr m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188 ' I ' ’ / I ' 1 i ' Pt ^i1 1 ' 1 I r 1 1 1 I 1 22.40 22.60 22.80 23.00 23.20 5000 m/z 189.10 14.20%

80 94 160 66

m/z-> 0 TTTTTTTTTTTTTTT 40 50 60 70 80 p .....I..... 'W... 90 100 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 10.90% ft 5000

66 80 T 0 TPPTPTTPTTPTIPIP*IPILTTT 158 TTT /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

307 .D SCAN508 .M Wed Jan 09 15:16:57 2002 Page 12

NYC-WTC_000051070

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NYC-WTC_000051070Source: NYC Law Department, mirrored locally

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