GCMS analysis results, sample AE00703, January 2002

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Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.

NYC-WTC_000051842–000051859

Folder label: “GCMS X 1/10/02 A 1/16/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN16\00703 .D Vial: 3 Acq On : 16 Jan 2002 4:47 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N. L ********************************************************* * * *** * * * * * * * Peak Number 9 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.27 ug/L 160372 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

I DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 94 2 Anthracene-dlO- 188 C14D10 001719-06-8 91 3 Phenanthrene-diO 188 C14D10 001517-22-2 64 4 Acridine-D9 188 C13D9N 000000-00-0 64 Abundance Scan 1699 (22.771 min): 00703.D (-) m/z 188.10 100.00% 188

5000

80 94 1 i 1 । 1 ■ i ■ ’ ■ T > . 11 i. । । > 40 52 66 । 146 160 22.40 22.60 22.80 23.00 23.20 0 TTT —PP —H I I | I I . I | | | I I I I | I f I I |T| B | n H | rr > rr | m/ Z 94.05 16.54% /z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 I mmmm । "I ri i , | , 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.05 16.05% 66 158 Of TTIUTTTWTTTTTTTT monf TmTPTTPTTTP mtz--> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188 . । . < , , । . I I TT I । r i । i . i . । , 22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 15.25%

66 80 94 | ' r* ri i rri ri | i i i i । I I i Of ' ' | ।'1111" • ■ ।" । m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 . । । । . r । r । i । . . । 1« । । -I 108 22.40 22.60 22.80 23.00 23.20 m/z 189.10 11.26% 5000

66 80| g4 7 160

n/z-> Oh mmpammmnmnmpr 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .. 1891 22.40 22.60 22.80 23.00 23.20

3703.D SCAN508.M Thu Jan 17 08:17:30 2002 Page 11

NYC-WTC_000051856

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NYC-WTC_000051856Source: NYC Law Department, mirrored locally

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