GCMS analysis results for sample AD31677, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN23\31677.D Vial: 2 Acq On : 23 Jan 2002 3:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C: \MSDCHEM\1 . . . \SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.34 ug/L 205090 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 94 2 Anthracene-D10 188 C14D10 000000-00-0 86 3 Phenanthrene-dl0 188 C14D10 001517-22-2 78 4 Anthracene-dlO- 188 C14D10 001719-06-8 64 Abundance Scan 1699 (22:771 min): 31677.D (-) m/z 188.15 100.00% KB

5000

80 94 66 22.40 22.60 22.80 23.00 23.20 54 0 i • ■• i ■1 ■ ■ i - i ■ ■" । ■ ■ ■ ■ । ■ i I " 1 *'11" 11111111 p —158 I m/z 94.10 18.20% z— > 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 ——ITTTmeTTIt 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.00 16.23% 158 . I 0 i■■■■i'■ “ i ‘ 66' i ■ ■' ■ T-TTTt 111'1111'11 rprev 1।11111111'| 11 > 111 > 11 -III/ > > > । miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 KB

2240 22.60 2280 23.00 23.20 5000 m/z 184.10 13.63% 80 94 66 160 ,| 111 mmHHWr /z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 KB 22.40 22.60 22.80 23.00 23.20 m/z 189.10 13.28%

5000

80 160

iz—> 0 mPmTT 40 50 60 66 94 i • • ■ ■ i ■ ‘ ■ i ■ ‘ 70 80 90 100 110 120 130 140 150 160 170 180 190 । l— ______ / • i • ’ • ■ i • ■1 “ i ■ ■ ■ • । ■ • • • । ■ 22.40 22.60 22.80 23.00 23.20

31677.D SCAN508.M Thu Jan 24 09:57:38 2002 Page 9

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