GCMS results for sample AE00314, Jan 24 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN14\00314.D Vial: 3 Acq On : 14 Jan 2002 12:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.30 ug/L 181744 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual I DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 94 2 Anthracene-dlO- 188 C14D10 001719-06-8 83 3 Anthracene-D10 188 C14D10 000000-00-0 72 4 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 Abundance Scan 1699 (22.771 min): 00314. D (-) m/z 188.10 100.00% 18 8

5000

80 94 22.40 22.60 22.80 23.00 23.20 40 66 146 158 — m/z 94.10 18.08% 0 .............. — i1 ■ ■ ■ i ■ ■ ■ ■ । ........ .1........ n/z-> 30 ■ i ■ ■ ■■ । ■ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 A Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 ‘i TT 22.40 22.60 22.80 23.00 23.20 80 94 m/z 189.15 15.71% 66 — 158 Or wuutt ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■1 ■ i ■ i''' ■ i ■' ■ ■ i'' " i ........ rn/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 80.10 13.64%

80 94 160 66 ok ■ । i111' i I "ill'"'I" >i■ i1111111" i11" r m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 r.... 188 22.40 22.60 22.80 23.00 23.20 m/Z 184.10 9.60%

5000 80 94 66 160 | Ok ■।>•••।■ — ' I " " 11 " 11 " 111'" " . ..... rl‘ fr^rr n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

00314.D SCAN508.M Tue Jan 15 08:47:52 2002 Page 11

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