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GCMS instrument data file SCAN508, Jan 31 2002

Machine-extracted title · confidence 90%

Instrument output file from GCMS analysis using method SCAN508 showing response for deuterated internal standards.

NYC-WTC_000052205–000052221

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052220
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NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02JAN31\00845.D Vial: 6 Acq On : 31 Jan 2002 6:51 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.38 ug/L 317627 Phenanthrene-dl0 22.65

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 87 2 Anthracene-dlO- 188 C14D10 001719-06-8 78 3 Anthracene-DlO 188 C14D10 000000-00-0 59 4 Cycloheptanone, 4-phenyl-188 C13H160 067688-28-2 50 Abundance Scan 1699 (22.771 min): 00845.D (-) m/z 188.15 100.00% 188

5000

94 . । , . . , । , r, ~ l . , । । । , . , , । . 80 22.40 22.60 22.80 23.00 23.20 43 52 66 132 158 | 0 ., 111 rrll . 11111 -+++- ----- TTTT7 m/ z 94.10 18.56% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z189.20 14.75%

n/z-> 66 o1 ■ ■ i ■r ■ ■ i ■ ■»■ । < l. ।. THT TTTf mmTTPTTTHTTT 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 —l Abundance #84502: Anthracene-d10- 188 ............ ....... ..... ...........................

22.40 22.60 22.80 23.00 23.20 5000 m/ z 184.10 11 62%

80 94 160 , . 66 0‘i' 1111 >> । ■ TT rr 11*0—————— ‘I dl 180. । m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ... . . Abundance #84498: Anthracene-D10 188 22.40 22.60 22.80 23.00 23 20 m/z 80.10 10.51%

5000 80 94 66 160 O'. । ।।। I. । k TT TrTT ............................... ’ TPITT m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 2280 23.00 23.20

00845.D SCAN508.M Fri Feb 01 09:19:36 2002 Page 14

NYC-WTC_000052220

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NYC-WTC_000052220Source: NYC Law Department, mirrored locally

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