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GCMS analysis results for sample AD31639, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31639 including unknown compounds and surrogate recovery data.

NYC-WTC_000049957–000049974

Folder label: “GCMS X 1/3/02 A 1/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C : \MSDCHEM\1\5973N\02 JAN1731639 .D Vial: 2 ‘ Acq On : 17 Jan 2002 3:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.32 ug/L 194805 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-dlO- 188 C14D10 001719-06-8 87 3 Anthracene-D10 188 C14D10 000000-00-0 83 4 Phenanthrene-diO 188 C14D10 001517-22-2 78 Abundance Scan 1699 (22.771 min): 31639.D (-) m/z 188.20 100.00% 1(0

5000

94 66 80 22*40 22.60 22.80 23.00 23*20 43 0- ‘' I ■ ‘ “ 11 1 > ■ j * • 111 >' 111»*»»IH'm156 I’r T’’ m/z 94.10 18.97% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 189.10 14.47% 66 1 158 ■" ■ i' 1 ■ i" ■11" " i" " i'1 ■' i" " i “1H " ■' । ■' ■■ ।1 All " " 0- ■■i" " i ■ ।। ■ i ■■1 ■

miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188 - 22.40 2260 22.80 23.00 23.20 5000 m/z 80.10 13.04%

niz-> 0 40 50 60 6 4 70 80 160 -------- . I, 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 ______/ —mmgT ■ i ■ ■ ■ ■ i ■ 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 12.67%

5000 80 94 66 160 1 m/z—> 0 mm ‘ 1 mHmmmlm 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

31639.D SCAN508.M Tue Jan 22 08:37:09 2002 Page 6

NYC-WTC_000049966

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NYC-WTC_000049966Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.994

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