GCMS analysis results for sample AD31639, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31639 including unknown compounds and surrogate recovery data.

NYC-WTC_000049957–000049974

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN17\31639.D Vial: 2 Acq On : 17 Jan 2002 3:39 pm . Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3' 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.15 ug/L 89830 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 47 3 3-Cyanocarbazole $$ 9H-Carbazole. .. 192 C13H8N2 057102-93-9 45 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 42 Abundance Scan 1656 (22.280 min): 31639.D (-) m/z 192.10 100.00% 1512

5000

82। 96 146 160 110 118 i 22.00 22.20 22.40 22.60 44 64 . 0- MTTFTTpeemi 111111.111111 n 111'1. । mmTTTP ' ‘ I “ “ I ‘1'11 Ip m/z 191.10 17.56% /z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-.BETA-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000 108 ) ■ ■ i • * ■ ■ i ■ ■ ‘ ■ i ■ ■ 22.00 22.20 22.40 22.60 A 146 175 m/z 96.10 14.35% 0 “ ’ I *' “ I • “ • I * hairrn [1 l t I 1 I * I “ ’ ‘ I “ * ‘ I 1 u 11 ’ “ U “ “ P *1 • P ‘ I • • • • I ‘ “ I ‘ ‘ m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 77 151 130 22.00 22.20 22.40 22.60 93 104 m/z 146.10 13.76% 5000 119

177 0 '‘‘I‘ ‘‘I"'' I‘ 'I'‘‘ 'I'‘‘>I ‘“I‘ -rp-rr I “ " “ ' I 1 ■।■■••।•■■•। । ‘ । '''441 iz—> Abundance 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192 ASmmm 22.00 22.20 22.40 22.60 m/z 160.10 11.56%

5000

96 164 138 0 1‘11101111111911111701102/1111/1/113011112"3TT2311‘‘"‘1-"‘h5 ■i. ।11... i1 113111 n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22,20 22.40 22.60

31639.D SCAN508.M Tue Jan 22 08:37:08 2002 Page 5

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