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GCMS results for sample AE00321, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00321 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051394–000051407

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051406
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00321.D Vial: 2 Acq On : 11 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

22.77 0.29 ug/L 171445 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 90 2 Anthracene-diO- 188 C14D10 001719-06-8 83 3 Phenanthrene-dlO 188 C14D10 001517-22-2 72 4 Acridine-D9 188 C13D9N 000000-00-0 72 Abundance Scan 1699 (22.771 min): 00321.0 (-) m/z 188.15 100.00% 188

5000

80 66 156 22 40 22.60 22.80 23.00 23.20 49 0 '' r r ■ ''r ■ ■ ■ i - । ■ i • ■ ■ • i I "I I mopprer TTT m/z 189.20 19.62% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 108

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/ z 80.05 15.06% 66 158 Ot TTTUTTTITTTTTTTTT 11111' 1111" " i"ri i1111111111"111ri 1H111 all. n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188

22.40 22.60 22.80 23.00 23.20 5000 m/ z 94-10 13.59%

— 80 94 DO | 160 , । n/z-> 0 —mPTTT 1..... W1... 1' r ' ■111' " r ' ■ ’ i " ■' i' 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 ■ । ■ ■ ■ ■ । TT 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 10.92%

5000

80 94 160

m/z-> 66 0 mPPTPTT - 40 50 60 - 70 80 90 100 110 120 130 140 150 160 170 180 190 -19— ■ i ■ ■ T' 1 ' ' I ' 4 ‘ ' I ' 22 40 22.60 22.80 23.00 23.20

00321.D SCAN508.M Mon Jan 14 10:46:43 2002 Page 9

NYC-WTC_000051406

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NYC-WTC_000051406Source: NYC Law Department, mirrored locally

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