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GCMS results for sample AE00739, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051967–000051983

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051981
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN16\00739.D Vial: 7 Acq Gn : 16 Jan 2002 8:07 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 9 Phenanthrene-dlO Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.37 ug/L 236093 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 86 2 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 83 3 Anthracene-dlO - 188 C14D10 001719-06-8 56 4 Anthracene-DlO 188 C14D10 000000-00-0 50 Abundance Scan 1699 (22.771 min): 00739.D (-) m/z 188.10 100.00% 188

5000

94 ■ I ' ' ' ‘ I 1PPT ' ' ' ' i . ........ — 80 22.40 22.60 22.80 23.00 23.20 43 66। 146 160 I | 0- 111'''1' i1' ‘11' -HH —TTTTTTT m/z 94.05 16.16% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188

5000 . | 1 . . . । .r .- . 22.40 22,60 22.80 23.00 23.20 m/z 189.15 12.55% 80 94 160 66

/z-> 0 TIPPPTTTTTT -HI— - ...... . 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ......... Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-dlO 188 ---------------------------- 22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 11.99% fl 80 94 66 I 158 01.111 ■ । । ■ 1111 > -HP '' " I' " I n 1' r 1'11" " i11 "'I'1111' rl'H ।11111111111'^1 niz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 - Abundance #84502: Anthracene-d10- 188 22.40 22.60 22.80 23.00 23.20 m/z 80.10 11.23% 5000

rk 80 94 160 , .

n/z-> 0 Ill..... 189... 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 - rr n Pm) 22.40 22.60 22.80 23.00 23.20

0739.D SCAN508.M Thu Jan 17 08:17:53 2002 Page 11

NYC-WTC_000051981

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NYC-WTC_000051981Source: NYC Law Department, mirrored locally

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