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GCMS results for sample AE00739, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051967–000051983

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

blDIdLy earcn compound Keporc

Data File : C:\MSDCHEM\1\5973N\02JAN16\00739.D Vial: 7 ’ Acq On : 16 Jan 2002 8:07 pm Operator: Sample : 508scan Inst : Instrumen Mise 2002 : January 16, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ******************************************************************** * Peak Number 10 Decanedioic acid, bis(2-eth... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.41 6.95 ug/L 3449450 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhex... 426 C26H50O4 000122-62-3 94 2 Decanedioic acid, bis(2-ethylhex... 426 C26H50O4 000122-62-3 91 3 2-cyanomethylene-3-oxo-1,2,3,4-t... 185 C10H7N3O 000000-00-0 50 4 1-[4-[3-(2-chloro-9H-thioxahthen... 442 C24H27C1N2O2S 000000-00-0 47 Abundance Scan 2631 (33.411 min): 00739.D (-) m/z 185.10 100.00% 185

57 5000 112 ... I 83

n/z-> 0 a41 143 166 - IWIWm] 203_______ 268 40 60 80 100120140160180200220240260280300320340360380400420 297315 33.00 33.20 33.40 33.60 33.80 m/z 57.10 49.60% Abundance #345442: Decanedioic acid, bis(2-ethylhexyl) ester (CAS) $... 185

5000 57 ' T' 1 ' ' I " i r । । । । i । i । । । |-i । 112 33.00 33.20 33.40 33.60 33.80 m/ z 71.10 36.03% 83 143 166 203 2983i6 ! । il ii 0- " ■ i" ■ TT 1 l""l""l <... । r..11126811112111121111211112214128118211118141208111111110011111 n/z-> 40 60 80 100120140160180200220240260280300320340 360380400420 Abundance #345443: Decanedioic acid, bis(2-ethylhexy!) ester $$ Seba... 185 i ' ■ ■ 1 i ' 1 . 33.00 33.20 33.40 33.60 33.80 5000 112 m/z70.10 32.97% 71

mlz-> 0 +-xAM.... +268, .4.I,. 143 166. 203

40 60 80 100120140160180200220240260280300320340360380400420 297315 408426 ' i " '' i" " i" " I" " i '

Abundance #93917:2-cyanomethy lene-3-oxo-1,2,3,4-tetrahydroquinoxaline ' ' I ‘ ‘ 1 1 I ' 185 33.00 33.20 33.40 33.60 33.80 m/Z 112.10 31.55%

5000 157

90

m/z-> 0 .......11131 40 60 80 100120140160180200220240260280300320340360380400420 33.00 33.20 33.40 33.60 33.80

)0739.D SCAN508.M Thu Jan 17 08:17:53 2002 Page 12

NYC-WTC_000051982

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NYC-WTC_000051982Source: NYC Law Department, mirrored locally

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