GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
NYC-WTC_000051967–000051983Folder label: “GCMS X 1/10/02 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02JAN16\00739.D Vial: 7 . Acq On : 16 Jan 2002 8:07 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Thiocyanic acid, 2-benzothi... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 95686 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 59 2 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 58 3 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 56 4 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 Abundance Scan 1656 (22.280 min): 00739.D (-) m/z 192.10 100.00% 192
5000
- 'I" 1 ' I ' 1 82 96 146 160 22.00 22.20 22.40 22.60 49 66 120 । | || 0 TTT+ PPPPTPP r m/z 191.10 16.17% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102098: Thiocyanic acid, 2-benzothiazolyl ester (CAS) $$ ... 192
5000 22.00 22.20 22.40 22.60 m/z 193.10 14.91% “8290 108 122 134 148 160 0 ' ' ‘ I ' “ ' I 1 ‘ ‘ I 1 1 11 । । I । | I . u | . • । । । .. । I | n i i | I i I | | I I i i | i i | I | i I । I | | i'I i । i ! i i । i ! i i । n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... 192 p .rigi.— 22.00 22.20 22.40 22.60 5000 m/z 146.10 12.71%
91 165 131 147 119
mfe-> 0—PPTPTT 111'' I II 1Q I ' I • ■ ।' ।' ।'' । | i ■''1 ■' 11' 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Z Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS ............ A ■ 1 i » < ' * i * • ■ > i ■ 192 22.00 22.20 22.40 22.60 m/z 96.00 11.82%
5000
96 164
■n/z--> 0 —mmmmmPImPTT | 1113 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 138 l 22.00 22.20 22.40 22.60
30739.D SCAN508.M Thu Jan 17 08:17:53 2002 Page 10
NYC-WTC_000051980
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NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051860
GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051895
GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051948
Gas chromatography-mass spectrometry analysis of sample AE00738 conducted on 1/29/02, detecting unknown compounds and 2,4-DDD surrogate at 99 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050596
Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000051782
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051783
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 10 and 16, 2002.
Filed in the same folder
NYC-WTC_000051785
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051789
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
Filed in the same folder