Laboratory report documenting GCMS analysis of sample AD31646 with detection of unknown compounds and surrogate recovery.
NYC-WTC_000050240–000050257Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN22\31646.D Vial: 2 Acq On : 22 Jan 2002 1:02 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 N-perdeuteriobenzylideneani ... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 70052 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 53 3 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 49 4 Phenanthrene, 3-methyl- (CAS) $$♦.. 192 C15H12 000832-71-3 42 Abundance Scan 1656 (22.280 min): 31646.D (-) m/z 192.10 100.00% 192
5000 / k j \ • > I > • . • I J > • • 1 • . . ■ j ■ I p 82 96 146 160 । 22.00 22.20 22.40 22.60 44 66 । 1111111111111 > 11 ■ 11111 p-n !•] n Ii11111111.11111111 > > i m/z 191.10 18.22% Th’ n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 1512
5000 82 ...... II.... A, 22.00 22.20 22.40 22.60 54 110 m/z 193.10 14.35% 30 1 94 160 Tpmpe 11111 ■11 ‘ mMp WIIpmgut ’ ’I* m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102735:3-(2-Methoxy-5-methylpheny[)acrylic acid 161 192
22.00 22.20 22.40 22.60 5000 m/z 146.10 13.11% 77 132 103 . 145 ।।।।।। A111 > 1111111111 11111'1111"11 ... A.... I 1 1 1 1 175 1 111,1 1 1 " 1 1 — m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 19/2 A 22.00 22.20 22.40 22.50 77 151 m/z 96.00 12.95% 130 N 93 104 5000 119
177 . 11111 > • j । •11j•>11111 >11<।A ।.... । I* ’ ’1’ '111111" “‘l* • • | • I r TI miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60
31646.D SCAN508.M Thu Jan 24 13:55:35 2002 Page 11
NYC-WTC_000050254
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NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051642
Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050334
Laboratory report for sample AD31677 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050222
Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051567
Laboratory report showing GCMS analysis results for sample AE00562 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052108
Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051984
GCMS analysis log for sample AE00740 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051364
Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050664
Laboratory report listing unknown compounds and surrogate recovery for sample AE00165 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder