GCMS analysis results for sample AE09571, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050902\9570.D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 20 4,7-Ethanoisobenzofuran-l,3... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 33.31 2.41 ug/L 3395440 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4,7-Ethanoisobenzofuran-l, 3,5,8(... 208 C10H8O5 006537-90-2 14 2 2-Phenyl-3-methyl-pyrrolo (2,3-b)... 209 C13H11N3 1000147-66-7/9 3 Bicyclo[3.2.2]non-3-en-2-one, 8,... 150 C9H10O2 1000155-95-4 9 4 2-Chloroethanol 80 C2H5C1O 000107-07/3 9 Abundance Scan 5146 (33.315 min): 9570.D (-5144) (-) m/z 43.10 100.00% 43 109 178 too Iy-w""MeAon,,, 182 208 5000 66 85 149 240 98 125 138 ■ 1 i ■ ■ ■ ■ i ■ ■ 1 1 i ■ ■ ' ■ i

Of I ’ ' J 144 33.00 33.20 33.40 33.60 m/z 109.10 72.23% mfz~> 20 40 60 80 100 120 140 200 160 220 180 240 Abundance #126496:4,7-Ethanoisobenzofuran-1,3,5,8(4H)-tetrone, tetr... 66 208 WwSmv 94 5000 79 162 33.00 33.20 33.40 33.60 43 55 110 135 180 m/z 178.10 59.82%

O+tIid ,,. 4 lil , 4l, ll, , ।. +141..... r * n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #85120:2-Phenyl-3-methyl-pyrrolo(2,3-b)pyrazine 208

33.00 33.20 33.40 33.60 m/ Z 192.10 54.18%|

■ 5000

132 78 115 154 ih 181 0 i 1 ■ ■ 1 i 1 ■ 1 1 i ■ ■ n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #50: Bicyclo[3.2.2]non-3-en-2-one, 8,9-epoxy- 27‘ 39 53 66 81 94 33,00 33.20 33.40 33.60 m/ Z 2 08.00 51.47%|

5000 150

122

m/z-> 0 Tnf 20 —ll— 40 60 80 +97413-- 100 120 140 160 180 200 220 240 TT TIT 33.00 33.20 33.40 33.60

9570.D 050102 .M Mon May 13 11:46:50 2002 Page 26

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