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GCMS analysis results for unknown compounds, sample AE09093, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE09093 on May 10, 2002.

NYC-WTC_000044902–000044925

Folder label: “GCMS X 4/30/02 A 5/8/02

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OCR text

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\9093 .D Vial: 15 Acq On 9 May 2002 2:49 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 15 Bendazol Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 39.82 0.30 ug/L 233585 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Bendazol 208 C14H12N2 000621-72-7 9/ 2 .gamma.-Cyano-3-methyl-5,10-dihy. . . 208 C14H12N2 1000213-00-87 3 2-Propen-1-one, 1,3-diphenyl-, (E)- 208 C15H120 000614-47-1 7 4 Pyrazolo[5,1-c][1,2,4]triazine, ... 208 C9H9FN40 006763-70-8 7 Abundance Scan 6252 (39.813 min): 9093.D (-6251) (-) m/z 2 0 7.00 10 0.0 0 % 207 429

5000 84 148 283 pwpAr i1 11 11 356 39.4039.5039.6039.7039.8039.90 0- “T" 1 ' 11 ' I [ I I I I I I I T I I I 1 "i 1 Ti ' m/Z 429.10 98.62% m/z-> 50 100 150 200 250 300 350 400 Abundance #84873: Bendazol 207

5000 1 ' 1 1 1 1 ' 1 1 1 I I I 1 I II I I I I I I

39.4039.5039.6039.7039.8039.90 — 65 91 m/z 147.95 73.45%

m/z-> Abundance 0- ,1 ,1 ,r1, 1 j ,4 । 1 131 152 180 50 100 I I /*

150 I 1 I

200 I

207 I I

#84850: gamma.-Cyano-3-methyl-5,10-dihydrobenzo(f]indolizine I I

250 I I I I I

300 I I

350 400 M 39.4039.5039.6039.7039.8039.90 5000 m/z 208.00 73.45% 103 51 77 128 151 180 J 0- i 44 J J I 14,4.4 1 Lt, 4 Ahi m/z-> 50 100 150 200 250 300 350 400 Abundance #85108: 2-Propen-1-one, 1,3-diphenyl-, (E)- '11'11 * n |T'।11111'' * -111 •11 - -111 77 208 39.4039.5039.6039.7039.8039.90 m/z.191.00 68.28% 103 131 5000 51 MAM) N 11/11 179

0 27 , 1 1 1 ,1,1521,1 + I I I I I I I I I I Tip Tttt m/z-> 50 100 150 200 250 300 350 400 39.4039.5039.6039.7039.8039.90

9093.D 050102.M Thu May 09 13:33:41 2002 Page 18

NYC-WTC_000044924

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NYC-WTC_000044924Source: NYC Law Department, mirrored locally

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