GCMS results sample AE08257, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08257.D Vial: 15 Acq On : 17 Apr 2002 9:01 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1\METHODS\041702SCAN . M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 12 Isobenzofuran-1,3-dione, 4,. Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

34.95 0.25 ug/L 235395 Perylene-dl2 34.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Isobenzofuran-1,3-dione, 4,5-dim... 208 C10H8O5 001567-56-2 37 2 Quinoline, 2-(1-methyl-lH-imidaz... 209 C13H11N3 002552-97-8 9 3 Nortrimipramine 280 C19H24N2 002293-21-2 9 4 Bendazol 208 C14H12N2 000621-72-7 7 Abundance Scan 5424 ( 34 948 min) 08257 D (-5423) (-) m/z 264.10 100.00% 40 204 207

5000 86 193 129 118 I 281 34 60 34 80 35 00 35 20 0^ ------ m/ z 40.00 97.56% 1 ' I ' 1 ' ' I ' ' ' ' I ' 1 1 1 I 1 r' ' I ' ' ' ' I ' ’ n/z- > 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #84979 Isobenzofuran-1,3-dione, 4,5-dimethoxy- 44 78 208 104 135 5000 65 34.60 34 8 0 35.00 35.20 122 163 -|79 150 m/ z 49.00 82.93%

n/z- > 01 —40l 60u At .4 T I 4 80 100 120 140 160 180 190 "T1 "‘P‘ 11 .... । 200 220 240 , 111 260 ।, 280 44 vhttpkM“MaM4l Abundance #85119: Quinoline, 2-(1-methyHH-imidazol-5-yl)- 208

34.60 34 80 35 00 35 20 5000 m/z 206.90 69.18% 77 128 155

n/z—> 0— 40 J144I 4-dpe91 ■102113 pli hi । al 12,1/188181193 |l "ArrwMW""W 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #85100. Nortrimipramine 193 208 34 60 34 80 35.00 35.20 m/z 2 08.00 51.22% 249 5000 234

/z- > 0.... ii 40 60 57 71 II/ . , , 80 85

100 — 115 130

120 140 160) 152 165 V9 IL 180 200 220 —

220 240 260 280

280 AAsBAAA-AMRMY 34.60 34 80 35.00 35.20

08257.D 041702SCAN.M Thu Apr 18 09:33:59 2002 Page 17

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