GCMS analysis results for sample AE12473, June 2002

NYC 9/11 Public Portal Document UJGL X OUaLUii topOULU RCDOL L

Data File : C:\MSDCHEM\1\DATA\052802\12473.D Vial: 11 Acq On : 28 May 2002 10:26 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 15 Isobenzofuran-1, 3-dione, 4,.. Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T.

34.86 0.23 ug/L 86298 Perylene-d12 34.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Isobenzofuran-1,3-dione, 4,5-dim... 208 C10H8O5 001567-56-2 12/ 2 3,5-Ethanoquinolin-10-one, decah... 207 C13H21NO 021041-42-9 9 3 Bendazol 208 C14H12N2 000621-72-7/7 4 Pyrazolo[1,5-a]pyridine, 3-methy... 208 C14H12N2 017408-32-/ 5 Abundance Scan 5409 (34,860 min): 12473.D (-5408) (-) m/z 207.00 100.00% 207 116 96 129 5000 44

miz-> O-T 20 40 84 • ■ । ■ ■ ■ ■ । 60 !k." i • ■ ■' । 80 100 120 140 160 180 200 220 ■1 ■ ।' ■ ■ ■ । ■ ■ • ■ । ■ ....... 265 ' i * ‘ ' 4 I * ' ' ' 1 1 * 240 260 34.60 34.80 35.00 35.20 m/z 115.80 69.63% Abundance #84979: isobenzofuran-1,3-dione, 4,5-dimethoxy- 44 73 2(18 104 135 / 5000 *14’** LU T 65 163 179 34.60 34.80 35.00 35.20 122 m/z 96.00 63.04% 150 I A MMj O- r ■ i i1 4 — Tr L■-'M‘Y' r 1, 193 193 •' । ■ ■ ■11 ■ ■ ■ ■ i ■ ■ A mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #84800:3,5-Ethanoquinolin-1 0-one, decahydro-1,7-dimethyl-... 164 207 "dd ’de • i • * 96 34.60 34.80 35.00 35.20 5000 m/z 129.30 58.45% 44 70 150 192 57 0-- 27 H X , 14 t 1 82 !I 108 122 136 , I 179 lhpaah , th —H , l PT it m/z—> Abundance 20 40 60) 80 100 120 140 160 180 200 ' I '

#84873: Bendazol 2017 220 240 260 _M 34.60 34.80 35.00 35.20 m/z 208.00 57.59% 5000

65 _ 91 103

/z—> OY 20 — ti 40 77 51 .1 116 — —167180193 . i 7.A.।. 152 —— 60 80 100 120 140 160 180 200 ' ’ I ' ’ ' ’ I * ‘ ‘ ‘ 220 240 260 ’ A 4lMB noywnrnreH 34.60 34.80 35.00 35.20

12473.D 052202.M Thu May 30 10:42:27 2002 Page 17

NYC-WTC_000014100