GCMS analysis results for sample AE12473, June 2002

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Data File : C:\MSDCHEM\l\DATA\052802\12473.D Vial: 11 Acq On : 28 May 2002 10:26 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L

Peak Number 14 Anthracene-dlO- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.29 ug/L 266976 Phenanthranerie-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 91X 2 Phenanthrene-diO 188 C14D10 001517-22-2 787 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 4 1,4-Naphthalenedione, 2-hydroxy-... 188 C11H8O3 000483-55-6 40 Abundance Scan 3401 (23.062 min): 12473.D (-3391) (-) m/z 188.10 100.00% 188

5000 ............ ............................. 94 ee 80 160 22.80 23.00 23.20 23.40 43 66 | n/z-> O-mpm ----- hmmmmmpm ।" " i 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 l m/z 189.10 18.52% Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 94.20 17.47% 80 94 160 ,| 17 30 42 52 66 niz-> .1 0 ■ i “' ■ i “ “ I “1' 111" 1111 mH# 11PN 108118 132 146 T 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 +.1791794) Abundance #79827: Phenanthrene-d10 188 . . .................. 22.80 23.00 23.20 23.40 5000 m/z 80.05 11.54%

80 94 160 30 42 52 66 m/z-> V il 108118 132 0 PPmPth 11111 |t j ll n h 11111111 j i { j 11 j 11111 pi i 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 146.,4..179179l,.. Abundance #79771:3-Amino-4-methyl-6-methoxyquindline • ■ i ■ ■ ' 1 i ■ 188 22.80 23.00 23.20 23.40 m/z 184.10 11.26% 145 5000

117 41 51 63 77 89 102 130 159 ipejiI11/) l... 173 i 6 'l""I""I" V II ' i ‘ 1 /z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 22.80 23.00 23.20 23.40

12473.D 052202.M Thu May 30 10:42:26 2002 Page 16

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