GCMS results sample AE08257, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08257.D Vial: 15 Acq On : 17 Apr 2002 9:01 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 13 2,4-Dicyanopyridine Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

35.02 0.22 ug/L 210975 Perylene-dl2 34.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,4-Dicyanopyridine 129 C7H3N3 029181-50-8 4 2 Benzenamine, 2,5-difluoro- 129 C6H5F2N 000367-30-6 2 3 3,4-Difluoroaniline 129 C6H5F2N 003863-11-4 2 4 Flucytosine 129 C4H4FN3O 002022-85-7 2 Abundance Scan 5436 (35 019 min) 08257 D (-5435) (-) m/z 40.00 100.00% 40

5000 118 259 193 132 34.60 34 80 35.00 35 20 35 40

n/z-> 01 ■ ■ । 20 > . . ... ... |. ..2°.** 40 60 80 100 120 140 160 180 200 220 240 260 281

280 m/z 259.10 42.83% Abundance #58357: 2,4-Dicyanopyridine 119

5000- 102 51 34 60 34 80 35 00 35.20 35.40 75 m/z 118.00 40.78% | 89 26 38 n/z-> 01 12 । 4.1^ , Ji 20 40 63 60 *H 80 ' ' I ‘ 1 ' ' I 1 ' ' ' I ' 1 1 ' I ' ' ' ' I ' ' 1 1 I 1 ' ' ' I ' ' ' 1 I ' ' ' ' I 1 1 100 120 140 160 180 200 220 240 260 280 Abundance #58345. Benzenamine, 2,5-difluoro- 119

34.60 K........... 34.80 35.00 35.20 35 40 5000 m/ z 51.10 33.81% 82 101

31 57 44 70 01 H‘17rH4+#4*k, 1 413, Aijiv n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #121827 3,4-Difluoroaniline 1 ’9 34.60 34 80 35.00 35 20 35.40 m/ z 12 9.40 31.56% 5000 102

28 51 65 82 ---- 1 i । rt hrH. i i । । i । i । । i i 0 ----- — T‘EETIIIEEU‘CSTTTEETS‘T‘T‘‘*T7---11‘1111UT /Z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34 60 34.80 35 00 35.20 35.40

08257.D 041702SCAN.M Thu Apr 18 09:33:59 2002 Page 18

NYC-WTC_000047924