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GCMS analysis results for unknown compounds, sample AE09093, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE09093 on May 10, 2002.

NYC-WTC_000044902–000044925

Folder label: “GCMS X 4/30/02 A 5/8/02”

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Scanned page image, NYC-WTC_000044923
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050802\9093.D Vial : 15 Acq On 9 May 2002 2:49 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 14 Butanedioic acid, bis(trime... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 39.79 0.43 ug/L 337039 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanedioic acid, bis(trimethyls... 262 C10H22O4Si2 040309-57-7 9 2 Silane, [[3,3-dimethyl-4-methyle... 282 C15H30OSi2 095798-07-5/9 3 Pyridine, 3,5-dichloro- 147 C5H3C12N 002457-47-8 7 4 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C10H32O4Si5 000995-83-5 7 Abundance Scan 6249 (39.796 min): 9093. D (-6237) (-) m/z 221.10100.00%

A /A 73 147 221

295 356 5000 96 267 ‘ I 1 1 1 1 1 1 1 I I I 1 Dti I 49 39.40 39.60 39.80_______ 0 11 r '1111 ■1 ■ i1''" i | i i i i | > i } | 1 ’ 1 | 1 1 1 1 | । । 1 1 | । । 1 । | I”। I I | 1 1 1 1 | 11 1 1 | 1 1 11 | ' । 1 1 ) 1 vo TT m/z 147.05 96.31% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #65866: Butanedioic acid, bis(trimethylsilyl) ester 147 73

5000 A। 39.40 39.60 39.80_______ 45 247 m/ z 73.10 95.92%

/V 28 129 172 218 I. 01 mrr r14,4,44 TTT TITTTTUTTIPITTP**1*P11NITTITTT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #26862: Silane, [[3,3-dimethyl-4-methylene-2-(trimethylsil... 73 MMMWMLAA 1 I ' ' ‘ I I I 1—1—1 I I I I k 39.40 39.60 39.80_______ 5000 m/z 356.20 49.32% 147 45 105 0+ 2711 189 1131 177123222 . ....... I I I I I ■ I I I I I I I > I I . If I ‘ t | i Tt i | I I i I | I I II | I I I i | i I r i | < r i t | | i i r | i i i > | I | I i | r | I | | i । i r | i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #66200: Pyridine, 3,5-dichloro- —-1 | I | ‘ | | i r 147 39.40 39.60 39.80_______ m/z 295.10 45.05% 112 5000 50 85

/z-> 0 -H Tt 11'1''I1'''1''1'1'11'111'11 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 1’7’’"’ । u 111111111 1 39.40 I I I 1 | 39.60 | . r—1—1 | 39.80 r

9093.D 050102.M Thu May 09 13:33:40 2002 Page 17

NYC-WTC_000044923

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