GCMS analysis results for sample AE12162, June 2002

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Laboratory report documenting GCMS analysis of sample AE12162 conducted on June 5, 2002.

NYC-WTC_000013643–000013665

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

i Data File : C:\MSDCHEM\l\DATA\052302\12162.D Vial: 15 Acq On : 23 May 2002 9:22 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 15 9H-Purin-6-amine, N-methyl-... Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

37.71 0.22 ug/L 60915 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 9H-Purin-6-amine, N-methyl-9-(tr... 221 C9H15N5Si 032865-83-1 7 2 1,3-Benzodioxole, 5-[3-acetamino... 221 C12H15NO3 1000124-33-0 4 3 2-(Trifluoromethyl)-7H-1,3,4-thi... 221 C6H2F3N3OS1 094605-13-7 4 4 2(1H)-Quinolinone, 4-phenyl- 221 C15H11NO 005855-57-2 4 Abundance Scan 5894 (37.710 min): 12162.D (-5884) (-) m/z 147.10 100.00% 14.7 221 73 49 5000 355 281 191 37.40 37.60 37.80 38.00 0-p + • i "■ ■ i■■ ■ ■ i'" ■ i•"■ i■"11■ “• i■1 “i•"‘i“1 ■ i■ ■" i'' " ii"“i‘■ i• m/z 221.10 95.90% n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #87924:9H-Purin-6-amine, N-methyl-9-(trimethylsily!)- 221

73 TBBmmBBTTT 5000 1 ‘ I ' ' ’ l ' 37.40 37.60 37.80 38.00 45 165 192 m/ Z 73.10 64.58% | i 99 122138 ।

unMislumid O-pnidm.-*==*dhttpHH “i•■■'i1■ ■11 ■ ■ ■ ■ i"i“i“i■ miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #87894:1,3-Benzodioxole, 5-[3-acetaminopropyl]- 221

135 162 37.40 37.60 37.80 38.00 43 73 m/z 207.00 63.13% 5000

91 119 178 204 O-pr —41—jLL TpHm ■ ■ i1 “ ■ i ■'" । । । । ■u ■ i' /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #87911:2-(Trifluoromethyl)-7H-1,3.4-thiadiazolo[3,2-A]pyr... 1 ■ ' i ■ ■ ■ ■ i ■ • ■ ■ i ■ ■ ■ • i ■ • ■ ■ i 221 37.40 37.60 37.80 38.00 m/z 49.00 52.05%

5000 193 40 r 68

m/z-> 0- pui + 1 100 127 I 163 I I 1’1111111111111117-111"1"111037T0’"’"IEETTUUEZITTTTIT 20 40 60 80 1(X) 120 140 160 180 200 220 240 260 280 300 320 340 360 IT ■ ' i ■ 37.40 37.60 37.80 38.00 ■ ‘ i ■ ' 1 ■ i' ■ • ■I

12162.D 052202.M Wed May 29 09:55:14 2002 Page 17

NYC-WTC_000013664

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NYC-WTC_000013664Source: NYC Law Department, mirrored locally

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