GCMS analysis results for sample AE11417, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052002\11417.D Vial: 7 Acq On : 20 May 2002 6:10 pm Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 3.60 0.38 ug/L 313357 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 91/ 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 3 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 28 4 Allyl mercaptan 74 C3H6S 000870-23-5 25 Abundance Scan 88 (3.596 min): 11417.D (-83) (-) m/z 74.00 100.00% 74

5000 82

35 47 3.20 A3.40 3.60 3.80 4.00 0 ............ । I ■ ............... ' . Il । । ____ _______ L m/z 82.00 49.80% ' 1 I ' ' ' ' I ' ■ 1 । ■ ■ ■ 1 । 1 1 ■ ■ । 1 ■ ■ 1 । m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 47 82 3.20 „N . . , S . ... 3.40 3.60 3.80 4.00 m/ z 76.00 37.02% 35

m/z-> ol .12.... 26.1—011/1 10 20 30 40 50 60 62...... 1 ' । I 1 1 1 ' I ' 70 80 T1l , 108 1 ' i ' 1 ■ ■ I 1 1 1 'J ' 1 1 1 i 90 100 110 Abundance #115342: Acetonitrile, dichloro- 7|4 35 ........ ............. ............................ 3.20 3.40 3.60 3.80 4.00 5000 82 m/z 84.00 34.87%

0+ ■ 1 i ■ ■ ' ' I 1 1 ' 1 I 1 47

Il40' ' I,50' . ...... . m80-1 IIa"FIIIIIII "hwymosu /z-> 10 20 30 60 70 90 100 110 Abundance #28312:3,3-Dichloropropyne 74 3.20 3.40 3.60 3.80 4.00 m/z 47.05 25.38% 5000 38 I 47 ) "/W/lakioo 0 281 , III 1 , , 153 60 —4 ■ ................ I 1 1 11 1 I 1 1 1 1 I ' ' 1 1 1 1‘III 82 108 1 i 1 ' ' 1 i 1 ' ■ ■ i ■ 1 1 1 i 1 1 1 1 i m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4.00

11417.D 050102.M Thu May 23 10:45:14 2002 Page 4

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