GCMS analysis results for sample AE06307, April 2002

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Laboratory report documenting GCMS analysis of sample AE06307 conducted on April 18, 2002.

NYC-WTC_000039373–000039383

Folder label: “GCMS X 3/18/02 A 4/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020408\6307.D vial: 15 Acq On 8 Apr 2002 11:54 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-diO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.14 0.12 ug/1 420206 Phenanthrene-dl0 30.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 Benzene, 1-(1-cyclohexen-l-yl) -4... 188 C13H160 020758-60-5 50 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 50 Abundance Scan 4776 (31.141 min): 6307. D (-4763) (-) m/z 188.10 100.00% 188

5000

80 94 • • । 1 ■ 1 ‘ i ■ 1 1 ■ । 1 1 1 1 । 1 1 1 1T 40 160 30.80 31.00 31.20 31.40 0 ■ i'" ‘ i1 ■ ■11" " I ■'" ।।■ i" - m/z .94.10 17.37% mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 30.80 31.00 31.20 31.40 m/z 189.10 15.32% 80 94 160 , . 66 17 30 42 52 0 11' " 11' ।' 1111" 1111111111 THH —H 108 118 132 146 "I1.............. 111'' 1111 ■ i ’1 46—44.170179 — m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ----- 30.80 31.00 31.20 31.40 5000 m/z 184.10 12.45%

80 94 160

mlz-> 0 30 42 52 66__ | 108 118 132 TTTTT I 1 i T { i i it | I i i i | ll n । il I r । i i TTtr t | l 1 " |' 1 T TTr i | r 11111 ■ | 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 146,44.170179— Abundance #79791: Benzene, 1-(1-cyclohexen-1-yl)-4-methoxy- 188 30.80 31.00 31.20 31.40 m/ z .80.10 12.39% 5000 160

91 115 129 145 173 41 51 65 7 m/z—> 0 P -। 1 102 - Wt | | । - 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 l 1 30.80 31.00 31.20 31.40

63 07.D SCANAPR0902.M Tue Apr 09 15:17:46 2002 Page 5

NYC-WTC_000039382

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