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GCMS analysis results for sample AE06307, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06307 conducted on April 18, 2002.

NYC-WTC_000039373–000039383

Folder label: “GCMS X 3/18/02 A 4/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\DATA\020408\6307 .D Vial: 15 Acq On 8 Apr 2002 11:54 pm Operator: McLean Sample 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 30.27 0.10 ug/1 344526 Phenanthrene-dl0 30.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 64 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 59 3 9H-Fluorene, 9-ethylidene- 192 C15H12 007151-64-6 36 4 Anthracene, l-methyl- 192 C15H12 000610-48-0 36 Abundance Scan 4627 (30.265 min): 6307.D (-4612) (-) m/z 192.10 100.00% 192

5000

96 146 160 30.00 30.20 30.40 30.60 0 m 40 p M J..... H I... m/z->_______ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.10 19.92% Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 192

5000 30.00 30.20 30.40 30.60 89 175 m/ z 193.10 13.84% 45 55 631 77 145 , . 97 105 117 135 O—TT 444444 HTTTpt 11 —II,Htt 11, 163 TT 111 +++ 11111 TT I miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192

30.00 30.20 30.40 30.60 5000 m/z 146.10 13.19% 7 45 I O2 , 122 69| 82 90 148 160 108 134 0 -...... ----- TT -IPH— 1•..... • • l' m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81028: 9H-Fluorene, 9-ethylidene- I ' ' 1 1 I ■ ■ । 1 ■ ■ ' i 1 ■ 192 30.00 30.20 30.40 30.60 m/z 96.10 11.91% A 5000 165

83 99 41 0 I I _________ I 1 ' r 1 I [ 1 f 1 I 1 1 1 1 I 1 mL ■ ।"1 ■ ।"'' ।'1111" " i"111" " i11" i T 111111111 TT-p- 1 1 1 1 ' ' ' I ' 1 I 1 ' 1 1 I 1 1 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.00 30.20 30.40 30.60

6307.D SCANAPR0902.M Tue Apr 09 15:17:43 2002 Page 4

NYC-WTC_000039381

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NYC-WTC_000039381Source: NYC Law Department, mirrored locally

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