GCMS sample analysis results, AE11799, June 3, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.

NYC-WTC_000012794–000012822

Folder label: “GCMS X 5-21-02 A 5-22-02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11799.D Vial: 6 Acq On : 22 May 2002 5:54 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e 2** Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library. : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.29 ug/L 343483 Phenanthranene-dl0 22.92 Hit# of 5 Tentative ID MW MolForm CAS# Qual . • 1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 59 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 50 3 (+)-Calycotomine 223 C12H17NO3 1000127-35-0 50 4 Phenanthrene, 3-methyl- 192 C15H12 000832-71/3 40 Abundance Scan 3312 (22.539 min): 11799.D (-3304) (-) m/z 192.10 0.00% 192

5000

on 96 146 160 1 1 ' ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । 22.20 22.40 22.60 22.80 '1 ‘ i1 ‘ ' i 40 54 66 82 i 118 । 10 01 mmmmthnmmpmHlmmmt m/z 191.10 20.18% mfz~> 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 192

5000 1 ■ i ■ ■ • • i ■ ■ ■ ■ । ■ ‘ ■ • i ■ 1 • ■ । 22.20 22.40 22.60 22.80 89 175 m/z 146.10 12.99% 63 117 145 45 44Llll+l++4 . , i. |*i'l > 11. 111111 m 111 > 1111111 rj 111111 4 105 117 111135 . । mr | 111 163 0- pt THH 4 mfz~> 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192 -A22.20 22.40 22.60 22.80 5000 m/z 96.00 12.94%

45 |f , , 90 T 122 134 148 160.. 0 m l........................ I Ji, J|.. 1, 11... |.. I > |. 111'l 11111111111 hl 11 ■ > i fn n tr#n > 111111 > 11 10210000100110170013 m/z-> 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #80989: (+)-Calycotomine 19/2 22.20 22,40 22.60 22.80 m/z 193.10 12.74% 5000

176 M 41 51 65 77 91 104 118 131 148 160 | | 205 223 0 TTTTTTTTTTTmThtpmtttpt pnpg iz-> 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 230 22.20 22.40 22.60 22.80

11799.D 052202.M Tue May 28 12:02:59 2002 Page 16

NYC-WTC_000012814

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.

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