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GCMS analysis results for sample AE06409, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06409 conducted on May 3, 2002.

NYC-WTC_000060295–000060304

Folder label: “GCMS X 3/18/02 A 4/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020409\6409.D Vial: 13 Acq On : 10 Apr 2002 2:20 am Operator: McLean Sample : 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e.

Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 * * * * * * *************************************************************** Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.14 0.22 ug/1 252818 Phenanthrene-dl0 30.91

Hit# of 5 Tentative ID . MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 86 2 Phenanthrene-dlO 188 C14D10 001517-22-2 78 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 64 .4 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 50 Abundance Scan 4775 (31.135 min): 6409.D (-4762) (-) m/z 188.10 TOOTO^ Its

5000 / (............................ ........ .......... .................... ,,,1,60.... |,||... 30.S0 31.00 31.20 31.40 m/z .94.1015.62% •n/z~> 10 20 30 40 50 60 70 SO 90 100110 120 130 140 150 160 170 160 190 Abundance! #79626: Anthracene-dl 0- Its

5000 30.S0 31.00 31.20 31.40 m/z 189.10 13.55% RK 60 94 150 I I, ,1?, ■ ■i ■, 111. ■, ■ 111 ■ ■ I, .'’.9° HH m, I H, I i ll,, l|,, ttZz-> 10 20 30 40 50 60 70 60 90 100 110 120 130 140 150 160 170 160 190 Abundance #79627: Phenanthrene-dlO 10s

y .8O 31.00 31.20 31.40 5000 m/z 184.10 12772%

AR 94 160 ...... I,,, 6°,,, 4,2 I I IJ ' I 108 118 , ,132 146 ,170179.[,|||1 ■T nZz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance . #79771: 3-Amino-4-methyl-6-methoxyquinoline I, 10s y).8O 3100 31.20 31.40 m/z 80.10 11.32% 145 5000

I mZz-> 10 20 30 40 50 60 70 so 90 100 110 120 130 140 150 160 170 160 190 30.S0 31.00 31.20 31.40

6409.D SC71NAPR0 902 .M Thu May 02 14:14:21 2002 Page 5

NYC-WTC_000060303

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NYC-WTC_000060303Source: NYC Law Department, mirrored locally

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