GCMS analysis results for sample AE06408, May 2002

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Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020409\6408.D Vial: 12 Acq On : 10 Apr 2002 1:24 am Operator: McLean Sample : 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.14 0.22 ug/1 273761 Phenanthrene-dl0 30.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-dlO 188 C14D10 001517-22-2 74 3 Pentacyclo[7.3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 72 4 Pentacyclo[8.4;0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 50 Abundance Scan 4775 (31.135 min): 6408.D (-4766) (-) m/z 188.10 100.00% 188

5000 J 1 80 94 ipn 30.80 31.00 31.20 31.40 40 I I 160 ' I'''' I " " I'''' I " '' I' I'' I'''' I'''. I'''' i " I' I''' ‘ I " '. I' " ' 11' T I m/z 189.1017.94% Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826; Anthracene-dlO- 1!!8

5000 I 30.80 31.00 31.20 31.40 m/z 184.10 16.72% RR 160 I,

mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 4ibundance #79827: Phenanthrene-dlO 1^ I ' ' ' ' I 30.80 31.00 31.20 31.40 5000 m/z ,94.10 13.82%

RR 94 160 30 42 52 66 J || 108II8 132 TyrTTTynT-rp-rTTjtTT-ry4dTTqTd4-rjTT44-{-n-rt-|44TT-|-rTTT]-TTT-rpTT^ Tife-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 (\bundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11)Jtelradeca... 1(18 30 80 31 00 31.20 31.40 m/z .80.10 13.36% 5000 79 91 67 Inc 131

nZ2-> I pA 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 II 1 30.80 31.00 31.20 31.40

6408.D SCANAPR0902.M Thu May 02 14:13:05 2002 Page 6

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