GCMS analysis results for sample AE06408, May 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020409\6408.D Vial: 12 Acq On : 10 Apr 2002 1:24 am Operator: McLean Sample : 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C : \MSDCHEM\1. . .\SC7kNAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.55 1.75 ug/1 1343470 1,4-Dichlorobenzene-d4 10.67 Hit# of 5 Tentative ID MW MolForm. CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 1000186-02-3 36 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Pentane, 3-methoxy- 102 C6H14O 036839-67-5 9 4 2-Hydroxy-2-methylbutanoic acid 118 C5H10O3 1000196-27-1 9 Abundance Scan 421 (5.553 min): 6408.D (-416) (-) 7)3

5000 43

Ti/z-> UU5 87 103 11 'T’ I" I " I 10 20 30 40 50 60 70 80 90 100-110 120 130 140 150 160 170 180 m/z 43.10 30.20% Abundance #25344: Acetic acid, 3-[1,31dioxolan-2-ylpropyl ester 7(3

5000 5 20 5.40 5.60 5.80 43 m/z 41710 12.24% 27 J] 55 87 113 131 174 I''''I'''' I''' ‘ I I'''' I TiZz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #857: N-Ethylformamide 3D 73 520 5.40 5.60 5.80 5000 m/z 45.10 10.96% 44 58

m/z-> JU At 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 I''" I

Abundance #25472: Pentane, 3-methoxy- 713 520 5.40 5.60 5.80 m/z 71.10 6.67% 5000 45

29 55 .. 101......... ■n/2-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 520 5 40 5.60 5,80

6408.D SC7kNAPR0902 .M Thu May 02 14:13:03 2002 Page 5

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